Skip to main content
SpringerLink
Log in

Synthesis and crystal and molecular structure of O,O-dimethyl(p-carboran-2-yl)phosphonate

  • Organic Chemistry
  • Published:
Bulletin of the Academy of Sciences of the USSR, Division of chemical science Aims and scope

Conclusions

  1. 1.

    The dimethyl ester of p-carboran-2-yl phosphonic acid (I) has been synthesized.

  2. 2.

    X-Ray Crystallographic analysis has shown that crystalline I possesses a weak CH... O=P hydrogen bond involving the CH grouping of the p-carborane ring.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Log in via an institution

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Institutional subscriptions

Similar content being viewed by others

Literature cited

  1. R. D. Green, Hydrogen Bonding by CH Groups, Macmillan, London (1974).

    Google Scholar 

  2. R. Taylor and O. Kennard, J. Am. Chem. Soc.,104, 5063 (1982).

    Google Scholar 

  3. A. I. Yanovskii, A. E. Kalinin, Yu. T. Struchkov, Z. G. Bykhovskaya, and I. L. Knunyants, Zh. Strukt. Khim.,22, No. 3, 125 (1981).

    Google Scholar 

  4. J. C. Calabrese, A. T. McPhail, and G. A. Sim, J. Chem. Soc. B, 282 (1970).

    Google Scholar 

  5. L. A. Leites, L. E. Vinogradova, L. I. Zakharkin, A. Novak, and Ya. Belok, Izv. Akad. Nauk SSSR, Ser. Khim., 696 (1980).

  6. L. A. Leites, L. E. Vinogradova, J. Belloc, and A. Novak, J. Mol. Struct.,100, 379 (1983).

    Google Scholar 

  7. A. I. Yanovskii, Yu. T. Struchkov, L. E. Vinogradova, and L. A. Leites, Izv. Akad. Nauk SSSR, Ser. Khim., 2257 (1982).

  8. V. N. Kalinin, Dissertation, Moscow (1976).

  9. L. Pauling, The Nature of the Chemical Bond, Ithaca Cornell Univ. Press, Ithaca, New York (1960).

    Google Scholar 

  10. R. K. Bohn and M. D. Bohn, Inorg. Chem.,10, 350 (1971).

    Google Scholar 

  11. V. S. Mastryukov, E. G. Atavin, A. V. Golubinskii, L. V. Vilkov, V. I. Stanko, and Yu. V. Gol'tyapin, Zh. Strukt. Khim.,23, No. 1, 51 (1982).

    Google Scholar 

  12. O. V. Dorofeeva, V. S. Mastryukov, A. V. Golubinskii, L. V. Vilkov, and A. Almenningen, Zh. Strukt. Khim.,22, No. 5, 51 (1981).

    Google Scholar 

  13. N. I. Kirillova, A. I. Klimova, Yu. T. Struchkov, and V. I. Stanko, Zh. Strukt. Khim.,17, 675 (1976).

    Google Scholar 

  14. A. I. Yanovskii, N. G. Furmanova, Yu. T. Struchkov, N. F. Shemyakin, and L. I. Zakharkin, Izv. Akad. Nauk SSSR, Ser. Khim., 1523 (1979).

  15. W. C. Hamilton, Acta Crystallogr.,8 199 (1955).

    Google Scholar 

  16. C. E. Nordman, Acta Crystallogr.,13, 535 (1960).

    Google Scholar 

  17. R. G. Gerr, A. I. Yanovskii, and Yu. T. Struchkov, Kristallografiya,28, 1029 (1983).

    Google Scholar 

Download references

Author information

Authors and Affiliations

  1. A. N. Nesmeyanov Institute of Heteroorganic Compounds, Academy of Sciences of the USSR, Moscow

    A. I. Yanovskii, Yu. T. Struchkov, V. Ts. Kampel, V. I. Bregadze, N. N. Godovikov & M. I. Kabachnik

Authors
  1. A. I. Yanovskii
    View author publications

    You can also search for this author in PubMed Google Scholar

  2. Yu. T. Struchkov
    View author publications

    You can also search for this author in PubMed Google Scholar

  3. V. Ts. Kampel
    View author publications

    You can also search for this author in PubMed Google Scholar

  4. V. I. Bregadze
    View author publications

    You can also search for this author in PubMed Google Scholar

  5. N. N. Godovikov
    View author publications

    You can also search for this author in PubMed Google Scholar

  6. M. I. Kabachnik
    View author publications

    You can also search for this author in PubMed Google Scholar

Additional information

Translated from Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, No. 10, pp. 2299–2302, October, 1986.

Rights and permissions

Reprints and permissions

About this article

Cite this article

Yanovskii, A.I., Struchkov, Y.T., Kampel, V.T. et al. Synthesis and crystal and molecular structure of O,O-dimethyl(p-carboran-2-yl)phosphonate. Russ Chem Bull 35, 2102–2105 (1986). https://doi.org/10.1007/BF00957533

Download citation

  • Received:

  • Issue Date:

  • DOI: https://doi.org/10.1007/BF00957533

Keywords

Search

Navigation