Conclusions
The heterocycle 2,9-dioxo-1,3,8,10-tetraoxa-2,9-dithiacyclotetradeca-5,12-diyne has a conformation of C2 symmetry in the crystal; the acetylene fragments intersect at an angle of 20.8°. The bond lengths and the endocyclic valence angles are close to their standard values.
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Literature cited
G. H. Petit, P. van Nuffel, C. van Alsenoy, et al., J. Am. Chem. Soc.,106, 6899 (1984).
W. Reppe, Ann. Chem.,596, 1 (1955).
R. Destro, T. Pilati, and M. Simonetta, Acta Crystallogr.,B33, 4447 (1977).
H. Irngartinger, Chem. Ber.,105, 1184 (1972).
H. Irngartinger, Chem. Ber.,110, 744 (1977).
H. Irngartinger and A. E. Jungk, Chem. Ber.,110, 749 (1977).
G. Lowe, S. J. Salamone, and R. H. Jones, J. Chem. Soc. Chem. Commun., 262 (1984).
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Translated from Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, No. 12, pp. 2750–2753, December, 1987.
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Kataeva, O.N., Litvinov, I.A., Naumov, V.A. et al. Molecular structure of 2,9-dioxo-1,3,8,10-tetraoxa-2,9-dithiacyclotetradeca-5,12-diyne. Russ Chem Bull 36, 2548–2551 (1987). https://doi.org/10.1007/BF00957231
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DOI: https://doi.org/10.1007/BF00957231