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Synthesis of 2-oxohexahydrothieno[3,4-d]imidazole derivatives

  • Organic Chemistry
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Bulletin of the Academy of Sciences of the USSR, Division of chemical science Aims and scope

Conclusions

We synthesized the cis-3- and 4-methyl-2-oxo-6-(σ-carboxybutyl) hexahydro [3,4-d]-imidazoles by the reduction of the 3- and 4-methyl-2-oxo-2,3-dihydro-6-(carboxybutyl)-1H-thieno [3,4-d] imidazoles with HSiEt3 in CF3COOH and subsequent alkaline hydrolysis of the intermediate methyl ethers.

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Literature cited

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Authors and Affiliations

  1. N. D. Zelinskii Institute of Organic Chemistry, Academy of Sciences of the USSR, Moscow

    S. I. Zav'yalov & O. V. Dorofeeva

Authors
  1. S. I. Zav'yalov
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  2. O. V. Dorofeeva
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Additional information

Translated from Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, No. 7, pp. 1634–1636, July, 1980.

The authors express their gratitude to Prof. A. Mark (France) for supplying the sample of 2-oxo-4-methyl-6-(6-carboxybutyl)hexahydrothieno[3,4-d]imidazole.

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Zav'yalov, S.I., Dorofeeva, O.V. Synthesis of 2-oxohexahydrothieno[3,4-d]imidazole derivatives. Russ Chem Bull 29, 1178–1180 (1980). https://doi.org/10.1007/BF00949179

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  • DOI: https://doi.org/10.1007/BF00949179

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