Conclusions
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1.
Some dialkyl phosphoramidates were prepared and characterized.
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2.
Chloral adducts of dialkyl alkylphosphoramidates were prepared and characterized.
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3.
Under the action of triethylamine dialkyl alkyl(2,2,2-trichloro-1-hydroxyethyl)phosphoramidates break down with formation of dialkyl alkylformylphosphoramidates.
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Translated from Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, No. 3, pp. 587–593, March, 1968.
We thank R. R. Shagidullin for valuable advice and help in the interpretation and discussion of the IR spectra.
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Nikonorov, K.V., Gurylev, É.A. & Chernova, A.V. Condensation of chloral with phosphoramidic esters, and some properties of the compounds obtained. Russ Chem Bull 17, 569–573 (1968). https://doi.org/10.1007/BF00911613
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DOI: https://doi.org/10.1007/BF00911613