Summary
Some 2,4- and 2,5-dialkyltetrahydrothiophenes were prepared by conversion of the corresponding tetrahydrofuran homologs into 1,4-dibromoalkanes and cyclization of the latter under the action of sodium sulfide into dialkyltetrahydrothiophenes.
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Shuikin, N.I., Bel'skii, I.F., Barkovskaya, L.Y. et al. Synthesis of 2,4- and 2,5-dialkyltetrahydrothiophenes. Russ Chem Bull 11, 1024–1028 (1962). https://doi.org/10.1007/BF00905227
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DOI: https://doi.org/10.1007/BF00905227