Conclusions
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1.
A method was developed for the synthesis of difficultly accessible 2,2,6,6-tetramethyl-1-piperidinols from stable nitroxides (piperidinooxy free radicals).
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2.
A method is proposed for the quantitative determination of nitroxides with the aid of their reactions with phenylhydrazine.
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Translated from Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, No. 5,pp. 891–896, May, 1966.
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Rozantsev, É.G., Golubev, V.A. Synthesis of heterocyclic analogs of hydroxylamine. Russ Chem Bull 15, 852–856 (1966). https://doi.org/10.1007/BF00849386
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DOI: https://doi.org/10.1007/BF00849386