Summary
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1.
We have developed a new, simple and rapid method for the simultaneous determination of silicon and phosphorus in organic compounds.
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2.
We have used amperometric titration to determine silicon and phosphorus.
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3.
The accuracy of the method is ±0.3/0.
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Literature cited
T. R. F. W. Fennell, and J. R. Webb, Talanta2, 389 (1959).
M. N. Chumachenko, M. O. Korshun, V. P. Burlaka, and V. N. Simonova, Dokl. AN SSSR,133, No. 1, 138 (1960).
M. N. Chumachenko and V. P. Burlaka, Izv. AN SSSR, Otd. Khim. n., 560(1962).
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Chumachenko, M.N., Burlaka, V.P. The decomposition of organic substances by metallic potassium part 4. A new method for the simultaneous determination of silicon and phosphorus. Russ Chem Bull 12, 2–4 (1963). https://doi.org/10.1007/BF00846939
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DOI: https://doi.org/10.1007/BF00846939