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The synthesis of 2-diazoperfluoropropane (bistrifluoromethyldiazomethane)

  • Organic and Biological Chemistry
  • Published:
Bulletin of the Academy of Sciences of the USSR, Division of chemical science Aims and scope

Summary

  1. 1.

    By reduction of 2-nitroperfluoropropane, we have obtained and characterized hexafluoroisopropylamine.

  2. 2.

    By nitrosation of hexafluoroisopropylamine, we have obtained 2-diazoperfluoropropane (bistrifluoromethyldiazomethane).

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Translated from Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, No. 5, pp. 926–928, May, 1965 Original article submitted August 28, 1964

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Mochalina, E.P., Dyatkin, B.L. The synthesis of 2-diazoperfluoropropane (bistrifluoromethyldiazomethane). Russ Chem Bull 14, 899–901 (1965). https://doi.org/10.1007/BF00845719

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  • DOI: https://doi.org/10.1007/BF00845719

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