Summary
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1.
The reaction of O,O-diethyl and O,O-dibutyl S-[(Ethoxydimethylsilyl)methyl] phosphorodithioaies with triethylsilanol proceeds with replacement of the silicon-attached ethoxy group by the triethylsiloxy group.
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2.
0,0-Diethyl and 0,0-dibutyl S-[(3,3,3-triethyl-1,1-dimethyldisiloxanylmethyl] phosphorodithioates were prepared and characterized for the first time.
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K. A. Andrianov and I. K. Kuznetsoya, Izv. AN SSSR, Otd. khim. n.,1961 1792.
K. A. Andrianov and I. K. Kuznetsova, Izv. AN SSSR, Otd. khim. n.,1962 456.
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Andrianov, K.A., Kuznetsova, I.K. & Pakhomova, I. Reaction of O,O-dialkyl S-[(Ethoxydimethylsilyl)methyl] phosphorodithioates with triethylsilanol. Russ Chem Bull 12, 448–450 (1963). https://doi.org/10.1007/BF00844399
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DOI: https://doi.org/10.1007/BF00844399