Summary
Crystals of (NH3OH)3GaF6 have been isolated from aqueous solution. The compound crystallizes triclinic, with cell parametersa=6.539(5) Å,b=6.924(5) Å,c=9.403(1) Å, α=87.01(9)°, β=83.98(8)°, γ=70.28(8)°. The thermal decomposition was studied by TG and DSC analysis.
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Literatur
Ebler E, Schott E (1908) J Pr Chem78: 340
Sahoo B, Patnaik D (1961) Curr Sci30: 293
Frlec B, Hyman HH (1967) J Inorg Nucl Chem29: 2124
Pintaric M, Milićev S, Volavsek B (1990) Monatsh Chem121: 357
Bajc I, Milićev S, Volavsek B (1992) Monatsh Chem123: 321
Ban I, Golic L, Milićev S, Volavsek B (1995) Monatsh Chem126: 1279
Schwarzmann S (1964) Z Kristallogr120: 286
Soldatov EN et al. (1978) Dok Akad Nauk SSSR241: 357
Meden A, Golic L, Siftar J (1992) Vest Slov Kem Drustva39: 319
Brauer G (1975) Handbuch der Präparativen Anorganischen Chemie, Bd 1. Enke, Stuttgart
Kristl M, Golic L, Volavsek B (1994) Monatsh Chem125: 1207
Furman NH (1962) Standard methods of chemical analysis, vol 1, 6th edn. Van Nostrand, Princeton, NJ
Pietzka G, Erlich P (1953) Angew Chem65: 131
Kolthoff IM, Sandell EB (1945) Textbook of quantitative inorganic analysis. Macmillan, New York
Ceh M (1967) Laboratorijski prirocnik. SKD, Ljubljana
Hall SR, Stewart JM (1990) Xtal 3.0 Reference Manual. Universities of Western Australia and Maryland Lamb, Perth
Larson AC (1969) In: Ahmed FR, Hall SR, Huber CP (eds) Crystallographic computing. Munksgaard, Copenhagen, pp 291–294
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Kristl, M., Volavsek, B. & Golic, L. Untersuchungen des Hydroxylammonium-Fluorogallats. Monatsh Chem 127, 581–586 (1996). https://doi.org/10.1007/BF00817249
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DOI: https://doi.org/10.1007/BF00817249