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Synthese, Kristallstruktur und Konformation von N2-Dibenzyl-N1-t-butoxycarbonylhydrazin

Synthesis, crystal structure and conformation of N2-dibenzyl-N1-t-butoxycarbonyl hydrazine

  • Organische Chemie Und Biochemie
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Monatshefte für Chemie / Chemical Monthly Aims and scope Submit manuscript

Summary

The synthesis and the crystal structure of N2-dibenzyl-N1-butoxycarbonyl hydrazine are reported. The compound was prepared from commercially availablet-butyl carbazate. It crystallizes in the triclinic space group P 1 witha=5.479(1) Å,b=9.559(1) Å,c=9.748(1) Å,a=63.81(1)°, β=87.52(1)°, γ=74.07(1) Å,Z=1,D=1.18 g/cm3. The structure was solved by direct methods and refined toR=0.0329.

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Authors and Affiliations

  1. Institut für Allgemeine Chemie, Technische Universität Łódź, PL-90-924, Łódź, Polen

    Zdzisław Gałdecki

  2. Institut für Physik, Technische Universität Łódź, PL-90-924, Łódź, Polen

    Bernard Luciak

  3. Institut für Organische Chemie, Technische Universität Łódź, PL-90-924, Łódź, Polen

    Adam S. Redliński, Krzysztof Kaczmarek & Mirosław T. Leplawy

Authors
  1. Zdzisław Gałdecki
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  2. Bernard Luciak
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  3. Adam S. Redliński
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  4. Krzysztof Kaczmarek
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  5. Mirosław T. Leplawy
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Gałdecki, Z., Luciak, B., Redliński, A.S. et al. Synthese, Kristallstruktur und Konformation von N2-Dibenzyl-N1-t-butoxycarbonylhydrazin. Monatsh Chem 122, 37–42 (1991). https://doi.org/10.1007/BF00815162

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  • DOI: https://doi.org/10.1007/BF00815162

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