Summary
Treatment of 2-phenoxypropionic acid with polyphosphoric acid gave substituted benzofuran-3-ones (2a–h), which were converted into 2,3,4-trihydrodibenzofuran-3-ones (4a–h)via the compounds3a–h.Clemmensen reduction of the compounds4a–h gave the 2,3,4-trihydrodibenzofuranes (5a–h).
Zusammenfassung
Behandlung von 2-Phenoxypropionsäure mit Polyphosphorsäure lieferte die substituierten Benzofuran-3-one (2a–h), welche über3a–h in die 2,3,4-Trihydrodibenzofuran-3-one (4a–h) übergeführt wurden. DurchClemmensen-Reduktion von4a–h wurden die gewünschten 2,3,4-Trihydrobenzofurane (5a–h) erhalten.
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Deshmukh, M., Kharade, D. & Shirke, S.D. A short synthesis of 2,3,4-trihydrodibenzofuranes. Monatsh Chem 125, 971–976 (1994). https://doi.org/10.1007/BF00812712
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DOI: https://doi.org/10.1007/BF00812712