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Polyfunctional macroheterocycles. 1. Synthesis of sulfur-containing macroheterocycles with endocyclic amido or sulfonamido groups

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Chemistry of Heterocyclic Compounds Aims and scope

Abstract

The reaction of 1,8-diamino-, 1,8-bis(2-carbomethoxyethylamino)-, and 1,8-bis(2-phenylethylamino)-3,6-dithiaoctanes and 1,2-bis(2-aminoethylthiomethyl)-4,5-dimethylbenzene with adipic, phthalic, and terephthalic acid dichlorides leads to the corresponding sulfur-containing macrocyclic diamines. Macrocycles that contain endocyclic sulfonamido groups are formed in the reaction of benzene-1,3-disulfonic acid dichloride with hexamethylenediamine and 1,8-bis(2-carbomethoxyethylamino)-3,6-dithiaoctane. The oxidation of 9,10-benzo-8,11-dioxo-7,12-bis-(2-carbomethoxyethyl)-1,4-dithia-7,12-diazacyclotetradec-9-ene with 30% hydrogen peroxide was studied.

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Authors and Affiliations

  1. Irkutsk Institute of Organic Chemistry, Siberian Branch, Academy of Sciences of the USSR, 664033, Irkutsk

    M. G. Voronkov, V. I. Knutov & M. K. Butin

Authors
  1. M. G. Voronkov
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  2. V. I. Knutov
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  3. M. K. Butin
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Translated from Khimiya Geterotsiklicheskikh Soedinenii, No. 7, pp. 995–998, July, 1988.

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Voronkov, M.G., Knutov, V.I. & Butin, M.K. Polyfunctional macroheterocycles. 1. Synthesis of sulfur-containing macroheterocycles with endocyclic amido or sulfonamido groups. Chem Heterocycl Compd 24, 820–823 (1988). https://doi.org/10.1007/BF00633185

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  • DOI: https://doi.org/10.1007/BF00633185

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