Summary
Two variable volume injection valves, equipped with bypass loops, have been developed, primarily to circumvent problems with matrix effects in high sensitivity FIA.
The application of a dual channel valve for simultaneous analysis, zone sampling and merging zones techniques is discussed.
Examples for on-line dilutions up to several thousand-fold and the direct determination of calcium in Kjeldahl digests using the zone sampling approach and a study of the interference of ascorbic acid on the Griess reaction for nitrite are presented. The application of “chasing zones” techniques by coupling a simple single channel valve in a new way is proposed.
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References
Möller J (1987) In: Analytiker Taschenbuch, Bd 7. Springer, Berlin Heidelberg New York Tokyo
Manual injection valves V-100/V-200. Tecator, Sweden
Tecator application note AN 48/82 and related subnotes
Bergamin H, Zagatto EAG, Krug FJ, Reis BF (1978) Anal Chim Acta 101:17
Mindegaard J (1979) Anal Chim Acta 104:111
Hansen EH (1983) Anal Chim Acta 148:111
Tecator application note AN 51/84
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Möller, J. New injection valves and their application in flow injection analysis. Z. Anal. Chem. 329, 685–687 (1988). https://doi.org/10.1007/BF00624775
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DOI: https://doi.org/10.1007/BF00624775