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Continuous reactor system of monosized colloidal particles

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Abstract

A reactor system, which continuously hydrolysed the metal alkoxide in an alcohol solution, was designed using an electromagnetic stirrer and an ageing tube. Several monosized colloidal particles were produced by this reactor system, which had high reproducibility and reliability for long-term production. The relation between powder characteristics and experimental parameters such as reagent concentration, mixing rate, ageing time, temperature, was investigated. These parameters had an effect on the particle size, size distribution, morphology and state of agglomeration. It is possible to control the particle size to between 0.1 and 1.0 μm by varying the experimental conditions. A narrower size distribution of powders was obtained by using an electromagnetic stirrer with greater flow rate. Physical and chemical properties of monosized colloidal particles obtained by this reactor were comparable to those of monosized colloidal particles obtained by the batch process.

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Authors and Affiliations

  1. Department of Materials Science and Engineering, Fukui University, 9-1, Bunkyo 3, Fukui-shi, 910, Fukui-ken, Japan

    Takashi Ogihara, Manabu Iizuka, Teruaki Yanagawa, Nobuo Ogata & Kokichi Yoshida

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  1. Takashi Ogihara
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  2. Manabu Iizuka
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  3. Teruaki Yanagawa
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  4. Nobuo Ogata
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  5. Kokichi Yoshida
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Ogihara, T., Iizuka, M., Yanagawa, T. et al. Continuous reactor system of monosized colloidal particles. J Mater Sci 27, 55–62 (1992). https://doi.org/10.1007/BF00553836

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  • DOI: https://doi.org/10.1007/BF00553836

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