Abstract
The micromechanics of indentation-induced flaws in monocrystalline silicon have been studied in relation to strength determination. In the first part, the evolution of the deformation-fracture pattern during contact with a Vickers pyramid is described. Emphasis is thereby placed on the vital role of the residual component of the elastic-plastic contact field in driving the cracks. In the second part, the response of the cracks in subsequent strength testing is followed. A precursor stage of stable growth is observed prior to attaining a failure configuration, consistent with augmentation of the applied tensile (flexural) loading by the residual contact component. No detectable slow crack growth due to environmental influence is found. Nevertheless, silicon is revealed as a material of extreme susceptibility to brittle fracture, with significant strength degradation from contacts on the microscale. The relevance of this brittleness to the mechanical behaviour of silicon components as a function of fabrication and prospective service conditions is discussed.
Similar content being viewed by others
References
B. R. Lawn and D. B. Marshall, J. Amer. Ceram. Soc. 62 (1979) 347.
C. P. Chen, “Fracture Strength of Silicon Solar Cells” (Jet Propulsion Laboratory Report 79-102, Pasadena, 1979).
A. Misra and I. Finnie, J. Mater. Sci. 14 (1979) 2567.
D. Haneman, W. D. Roots and J. T. P. Grant, J. Appl. Phys. 38 (1967) 2203.
B. P. Lemke and D. Haneman, Phys. Rev. B 17 (1978) 1893.
B. R. Lawn and M. V. Swain, J. Mater. Sci. 10 (1975) 113.
B. R. Lawn and T. R. Wilshaw, ibid. 10 (1975) 1049.
B. R. Lawn and E. R. Fuller, ibid. 10 (1975) 2016.
A. G. Evans and T. R. Wilshaw, Acta. Met. 24 (1976) 939.
D. B. Marshall and B. R. Lawn, J. Mater. Sci. 14 (1979) 2001.
D. B. Marshall, B. R. Lawn and P. Chantikul, ibid. 14 (1979) 2225.
B. R. Lawn, A. G. Evans and D. B. Marshall, J. Amer. Ceram. Soc. 63 (1980) 574.
B. J. Hockey, S. M. Wiederhorn and H. Johnson, in “Fracture Mechanics of Ceramics”, edited by R. C. Bradt, D. P. H. Hasselman and F. F. Lange (Plenum, New York, 1978) p. 379.
B. R. Lawn, D. B. Marshall, P. Chantikul and G. R. Anstis, J. Aust. Ceram. Soc. 16 (1980) 4.
V. G. Eremenko and V. I. Nikitenko, Phys. Stat. Sol. (a) 14 (1972) 317.
M. J. Hill and D. J. Rowcliffe, J. Mater. Sci. 9 (1974) 1569.
P. Humble and R. H. J. Hannink, Nature 273 (1978) 37.
B. R. Lawn, B. J. Hockey and S. M. Wiederhorn, J. Mater. Sci. 15 (1980) 1207.
K. E. Puttick and M. A. Shahid, Ind. Diamond Rev. (July, 1977) 208.
A. S. T. Badrick, F. Eldeghaidy, K. E. Puttick and M. A. Shahid, J. Phys. D: Appl. Phys. 10 (1977) 195.
H. Kotake and S. Takasu, J. Mater. Sci. 15 (1980) 895.
B. R. Lawn and A. G. Evans, ibid. 12 (1977) 2195.
J. Lankford and D. L. Davidson, ibid. 14 (1979) 1662.
B. R. Lawn, J. Appl. Phys. 39 (1968) 4828.
R. J. Jaccodine, J. Electrochem. Soc. 110 (1963) 524.
J. J. Gilman, J. Appl. Phys. 31 (1960) 2208.
C. St. John, Phil. Mag. 32 (1975) 1193.
C. P. Chen and M. H. Leipold, Amer. Ceram. Soc. Bull. 59 (1980) 469.
V. R. Howes, Glass Tech. 15 (1974) 148.
J. J. Petrovic, R. A. Dirks, L. A. Jacobson and M. G. Mendiratta, J. Amer. Ceram. Soc. 59 (1976) 177.
B. R. Lawn and D. B. Marshall, in “Fracture Mechanics of Ceramics”, edited by R. C. Bradt, D. P. H. Hasselman and F. F. Lange (Plenum, New York, 1978) p. 205.
M. V. Swain, unpublished work (1980).
Author information
Authors and Affiliations
Rights and permissions
About this article
Cite this article
Lawn, B.R., Marshall, D.B. & Chantikul, P. Mechanics of strength-degrading contact flaws in silicon. J Mater Sci 16, 1769–1775 (1981). https://doi.org/10.1007/BF00540623
Received:
Accepted:
Issue Date:
DOI: https://doi.org/10.1007/BF00540623