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Synthesis of 4-ethoxycarbonylmethyl-, 4-N-phenylcarbamoylmethyl-, and 4-carboxymethyl-1,3-dithiole-2-thiones and the corresponding 1,3-dithiolium salts

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Chemistry of Heterocyclic Compounds Aims and scope

Abstract

A method for the preparation of 4-ethoxycarbonylmethyl-, 4-N-phenylcarbamoylmethyl-, and 4-carboxymethyl-1,3-dithiole-2-thiones and the corresponding 1,3-dithiolium salts from γ-bromoacetoacetic ester, γ-bromoacetoacetanilide, and sodium tertbutyltrithiocarbonate was developed. The compounds were characterized by their IR and PMR spectra.

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Literature cited

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Authors and Affiliations

  1. Riga Polytechnic Institute, 226828, Riga

    O. Ya. Neiland, D. V. Bite & R. B. Kampare

Authors
  1. O. Ya. Neiland
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  2. D. V. Bite
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  3. R. B. Kampare
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Deceased.

Translated from Khimiya Geterotsiklicheskikh Soedinenii, No. 2, pp. 180–183, February, 1984.

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Neiland, O.Y., Bite, D.V. & Kampare, R.B. Synthesis of 4-ethoxycarbonylmethyl-, 4-N-phenylcarbamoylmethyl-, and 4-carboxymethyl-1,3-dithiole-2-thiones and the corresponding 1,3-dithiolium salts. Chem Heterocycl Compd 20, 144–147 (1984). https://doi.org/10.1007/BF00506282

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  • DOI: https://doi.org/10.1007/BF00506282

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