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Polyfunctional macroheterocycles

6. Crown ethers containing n and s with exocyclic methoxycarbonylethyl, hydroxy-, or sulfonatomethyl groups

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Chemistry of Heterocyclic Compounds Aims and scope

Abstract

Reaction of 1-phenethyl- and 1-methoxycarbonylethylaziridine with 2,3-dimercaptopropanol gives the corresponding N-substituted (4-hydroxymethyl-1,8-diamino)-3,6-dithiaoctanes. Reaction of aziridine and Us 1-substituted derivatives with 2,3-dimercaptopropanesulfonic acid gives the corresponding [1,10-diamino-3-oxa-4, 8-dithia-6-(2-aminoethylthio)]decane-4,4-dioxides. Treatment of them with sodium bicarbonate produces the corresponding sodium 2,3-bis(2-aminoethylthio)propanesulfonates. Cyclocondensation of certain synthesized diamines with adipic diazide produces 16-membered macroheterocycles with exocyclic methoxycarbonylethyl, hydroxy-, or sulfonatomethyl groups.

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Authors and Affiliations

  1. Irkutsk Institute of Organic Chemistry, Siberian Branch, Russian Academy of Sciences, Irkutsk

    M. G. Voronkov, V. I. Knutov & O. N. Shevko

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  1. M. G. Voronkov
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  2. V. I. Knutov
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  3. O. N. Shevko
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Additional information

For Communication 5, see [1].

Translated from Khimiya Geterotsiklicheskikh Soedinenii, No. 5, pp. 704–707, May, 1992.

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Voronkov, M.G., Knutov, V.I. & Shevko, O.N. Polyfunctional macroheterocycles. Chem Heterocycl Compd 28, 596–599 (1992). https://doi.org/10.1007/BF00475266

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  • DOI: https://doi.org/10.1007/BF00475266

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