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Determination of the three-dimensional structure of 1, 2-dimethyl-7-tert-butyldecahydro-4-quinolone by pmr spectroscopy

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Chemistry of Heterocyclic Compounds Aims and scope

Abstract

The three-dimensional structure of l, 2-dimethyl-7-tert-butyldecahydro-4-quinolone was analyzed completely by PMR spectroscopy with the aid of the “shift-reagent’ technique. The induced shifts are described by a pseudocontact model realized by means of a computer program.

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Literature cited

  1. I. Ya. Slonim and A. Kh. Bulai, Usp. Khim., 42, 1976 (1973).

    Google Scholar 

  2. H. Booth and D. V. Griffits, J. Chem. Soc., Perkin II, 2361 (1972).

    Google Scholar 

  3. A. A. Akhrem, L. I. Ukhova, and A. N. Sergeeva, Izv. Belorussk. SSR, Ser. Khim., No. 4, 46 (1975).

    Google Scholar 

  4. N. Bhacca and D. Williams, Applications of NMR Sectroscopy in Organic Chemistry, Holden-Day (1964).

  5. J. Lefevre and M. L. Martin, Org. Magn. Res., 4, 737 (1972).

    Google Scholar 

  6. J. W. Apsimon and H. Beierbeck, Tetrahedron Lett., No. 8, 581 (1973).

    Google Scholar 

  7. J. W. Apsimon, H. Beierbeck, and A. Fruchier, Can. J. Chem., 50, 2725 (1972).

    Google Scholar 

  8. N. S. Angerman, S. S. Danyluk, and T. A. Victor, J. Am. Chem. Soc., 94, 7137 (1972).

    Google Scholar 

  9. M. R. Willcott, R. E. Lenkinski, and R. E. Davis, J. Am. Chem. Soc., 94, 1742 (1972).

    Google Scholar 

  10. N. S. Bakhvalov, Numerical Methods [in Russian], Moscow (1975).

  11. D. Hudson, Statistics for Physicists [Russian translation], Moscow (1970).

  12. J. K. M. Sanders and D. H. Williams, J. Am. Chem. Soc., 93, 641 (1971).

    Google Scholar 

  13. R. H. Newman, Tetrahedron, 30, 969 (1974).

    Google Scholar 

  14. K. Tori, Y. Yoshimura, M. Kainosho, and K. Ajisaka, Tetrahdedron Lett., 1573 (1973).

  15. H. Booth and J. H. Little, 23, 291 (1967).

  16. C. S. Springer, D. W. Meek, and R. E. Sievers, Inorg. Chem., 6, 1105 (1967).

    Google Scholar 

  17. H. Hart and L. M. Love, Tetrahedron Lett., No. 7, 625 (1971).

    Google Scholar 

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Authors and Affiliations

  1. Institute of Bioorganic Chemistry, Academy of Sciences of the Belorussian SSR, Minsk

    A. A. Akhrem, T. E. Prokof'ev, A. S. Fridman, L. I. Ukhova & A. N. Sergeeva

Authors
  1. A. A. Akhrem
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  2. T. E. Prokof'ev
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  3. A. S. Fridman
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  4. L. I. Ukhova
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  5. A. N. Sergeeva
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Translated from Khimiya Geterotsiklicheskikh Soedinenii, No. 5, pp. 651–657, May, 1976.

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Akhrem, A.A., Prokof'ev, T.E., Fridman, A.S. et al. Determination of the three-dimensional structure of 1, 2-dimethyl-7-tert-butyldecahydro-4-quinolone by pmr spectroscopy. Chem Heterocycl Compd 12, 547–553 (1976). https://doi.org/10.1007/BF00470109

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  • DOI: https://doi.org/10.1007/BF00470109

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