Skip to main content
Log in

Study of growth dislocations in L-arginine phosphate monohydrate single crystals by chemical etching

  • Published:
Journal of Materials Science Aims and scope Submit manuscript

Abstract

The results of a study of the distribution of growth dislocations revealed on different faces of L-arginine phosphate monohydrate (LAP) crystals by selective etching in relation to the growth conditions of the crystals are described. It was found that (1) the dislocation density, ϱ, on a face is the highest in its central regions and depends on the supersaturation used for growth, and that (2) ϱ on different faces is different. The observations are discussed from the standpoint of the mechanism of generation of dislocations at the seed-crystal interface in the initial stages of regeneration of the seed and at the crystal-medium interface due to the formation of bunches of growth layers on the growing crystal faces during their development.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Similar content being viewed by others

References

  1. K. Aoki, K. Nagamo and Y. Iitaka, Acta Crystallogr. B 27 (1971) 11.

    Article  Google Scholar 

  2. D. Eimerl, S. Velsko, L. Davis, F. Wang, G. Loiacono and G. Kennedy, IEEE J. Quant. Electron. 25 (1989) 179.

    Article  CAS  Google Scholar 

  3. A. Yokotani, T. Sasaki, K. Fujioka, S. Nakai and T. Yamanaka, J. Crystal Growth 99 (1990) 815.

    Article  CAS  Google Scholar 

  4. G. Dhanaraj, T. Shripathi and H. L. Bhat, ibid. 113 (1991) 456.

    Article  CAS  Google Scholar 

  5. S. Amelinckx, “Direct Observations of Dislocations”, Supplement to Solid State Phy. 6 (Academic Press, New York, 1964).

  6. K. Sangwal, “Etching of Crystals: Theory, Experiment and Application” (North-Holland, Amsterdam, 1987).

    Google Scholar 

  7. K. Sangwal, R. Rodriguez-Clemente and S. Veintemillas-Verdaguer, J. Crystal Growth 78 (1986) 144.

    Article  CAS  Google Scholar 

  8. K. Sangwal, S. Veintemillas-Verdaguer and J. Torrent-Burgues, ibid., 154 (1995) 364.

    Article  CAS  Google Scholar 

  9. M. C. Robert and F. Lefaucheux, ibid., 65 (1983) 637.

    Article  CAS  Google Scholar 

  10. H. Klapper, in “Characterization of Crystal Growth Defects by X-ray Methods”, edited by B. K. Tanner and D. K. Bowen (Plenum, New York, 1978) p. 133.

    Google Scholar 

  11. J. N. Sherwood and T. Shripathi, J. Crystal Growth 88 (1988) 358.

    Article  CAS  Google Scholar 

  12. K. Sangwal and R. Rodriguez-Clemente, “Surface Morphology of Crystalline Solids” (Trans Tech, Zurich, 1991) Ch. 3.

    Google Scholar 

  13. A. A. Chernov, Sov. Phys. Uspekhi 4 (1961) 116.

    Article  Google Scholar 

  14. J. P. van der Eerden and H. Müller-Krumbhaar, Electrochim. Acta 31 (1986) 1007.

    Article  Google Scholar 

  15. K. Sangwal, S. Veintemillas-Verdaguer and J. Torrent-Burgues, J. Crystal Growth 155 (1995) 135.

    Article  CAS  Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Rights and permissions

Reprints and permissions

About this article

Cite this article

Sangwal, K., Veintemillas-Verdaguer, S. & Torrent-Burgués, J. Study of growth dislocations in L-arginine phosphate monohydrate single crystals by chemical etching. JOURNAL OF MATERIALS SCIENCE 31, 6299–6304 (1996). https://doi.org/10.1007/BF00354453

Download citation

  • Received:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/BF00354453

Keywords

Navigation