Summary
The theories of KRATKY, DEBYE and BUESCHE and POROD have been applied to evaluate macromolecular parameters which speak of the fine structural characteristics of raw silk — a natural polymer in the solid state. The small-angle KRATKY camera has been utilised for the measurements of the scattering intensities. The macromolecular parameters evaluated are the percentage of void (w1), the specific inner surface (O/V), length of coherence (1c), range of inhomogeneity (1r), transversal length −s − \(\bar l_l\) and \(\bar l_2\) which were found to be equal to 0.13%, 25.15 × 10−4 Å−1, 21.84 Å, 2.11 Å, 1.59 × 103 Å and 2.11 Å respectively The physical properties as evaluated by Scott's IP2 Tester have been reported.
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Patel, A., Padhl, R.C. & Labischinski, H. Fine structural characteristics and physical properties of raw silk. Polymer Bulletin 5, 437–441 (1981). https://doi.org/10.1007/BF00255980
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DOI: https://doi.org/10.1007/BF00255980