Abstract
The synthesis of beta-alumina powder from kaolin-derived aluminium sulphate solution is described. A homogeneous mixture of Al2(SO4)3·18H2O and Na2SO4·10H2O was precipitated by dropping the mixed solution of the kaolin-derived aluminium sulphate and sodium hydroxide into ethanol with agitation by stirring. The preparation conditions - mixing mole ratio of Na2O/Al2O3 in the solution and calcination temperature of the resultant precipitate — were experimentally determined for obtaining the beta-alumina powder with a structure consisting of β- and β″-alumina and a well crystallized state.
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Kang, H.K., Park, H.C. & Kim, K.H. Preparation of beta-alumina powder from kaolin-derived aluminium sulphate solution. J Mater Sci: Mater Electron 7, 385–389 (1996). https://doi.org/10.1007/BF00180774
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DOI: https://doi.org/10.1007/BF00180774