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Journal of Porous Materials

, Volume 25, Issue 5, pp 1359–1363 | Cite as

Direct synthesis of ordered mesoporous carbon applied in hydrogen storage

  • Juliana M. Juárez
  • Marcos Gómez Costa
  • Oscar A. AnunziataEmail author
Article

Abstract

In this work, we present a direct, novel and low cost method for the preparation of an ordered mesoporous carbon (OMC). OMC was successfully synthesized by the carbonization of the silica/triblock copolymer/sucrose composite in the presence of sulfuric acid. The resulting material was characterized by XRD, N2 sorption analysis and TEM techniques. The novel synthesis technique improved significantly the H2 storage properties (3.78 wt%) compared with that of CMK-3 synthesized using the nanocasting strategy (2.2 wt%) at 77 K and 10 bar.

Keywords

Carbon materials Hydrogen storage OMC Nanomaterials 

Notes

Acknowledgements

Juliana M. Juárez, Marcos Gómez Costa, Oscar A. Anunziata, NANOTEC, CONICET, National Technology University, Cordoba Faculty, Maestro Lopez y Cruz Roja Argentine. We acknowledge the financial support of CONICET Argentina, PIP CONICET 11220120100218CO. 2014 -2017.

References

  1. 1.
    K. Ariga, A. Vinu, Y. Yamauchi, Q. Ji, J.P. Hill, Bull. Chem. Soc. Jpn. 85, 1–32 (2012)CrossRefGoogle Scholar
  2. 2.
    S.H. Joo, S.J. Choi, I. Oh, J. Kwak, Z. Liu, O. Terasaki, R. Ryoo, Nature 412, 169–172 (2001)CrossRefPubMedGoogle Scholar
  3. 3.
    X. Jin, V.V. Balasubramanian, S.T. Selvan, D.P. Sawant, M.A. Chari, G.Q. Lu, A. Vinu, Angew Chem. Int. Ed. 48, 7884–7887 (2009)CrossRefGoogle Scholar
  4. 4.
    A. Vinu, P. Srinivasu, M. Takahashi, T. Mori, V.V. Balasubramanian, K. Ariga, Microporous Mesoporous Mater. 100, 20–26 (2007)CrossRefGoogle Scholar
  5. 5.
    A. Vinu, M. Miyahara, K. Ariga, J. Phys. Chem. B 109, 6436–6441 (2005)CrossRefPubMedGoogle Scholar
  6. 6.
    W. Zhuang, Y. Wan, C. Feng, Y. Shen, D. Zhao, Chem. Mater. 21, 706–716 (2009)CrossRefGoogle Scholar
  7. 7.
    T. Kyotani, T. Nagai, S. Inoue, A. Tomita, Chem. Mater. 9, 609–615 (1997)CrossRefGoogle Scholar
  8. 8.
    G. Che, B.B. Lakshimi, E.R. Fisher, C.R. Martin, Nature 393, 346–349 (1998)CrossRefGoogle Scholar
  9. 9.
    J.M. Juárez, M.B. Gómez Costa, O.A. Anunziata, Int. J. Energy Res. 39, 128–139 (2015)CrossRefGoogle Scholar
  10. 10.
    R. Liu, Y. Shi, Y. Wan, Y. Meng, F. Zhang, D. Gu, Z. Chen, B. Tu, D. Zhao, J. Am. Chem. Soc. 128(35), 11652–11662 (2006)CrossRefPubMedGoogle Scholar
  11. 11.
    A. Prabhu, A. Al Shoaibi, C. Srinivasakannan, Mater. Lett. 136, 81–84 (2014)CrossRefGoogle Scholar
  12. 12.
    J.M. Juárez, M.B. Gómez Costa, O.A. Anunziata, Int. J. Energy Res. 39, 941–953 (2015)CrossRefGoogle Scholar
  13. 13.
    V. Vallés, B. Ledesma, J. Juárez, M. Gómez Costa, O. Anunziata, A. Beltramone, Fuel 188, 155–165 (2017)CrossRefGoogle Scholar
  14. 14.
    U. Suryavanshi, T. Iijima, A. Hayashia, Y. Hayashi, M. Tanemura, Chem. Eng. J. 179, 388–393 (2012)CrossRefGoogle Scholar
  15. 15.
    F. Zeinaldi, A.A. Ghoreyshi, G.D. Najafpour, Middle East J. Sci. Res. 5(4), 191–198 (2010)Google Scholar
  16. 16.
    C. Liu, Y. Chen, C.Z. Wu, S.T. Xu, H.M. Cheng, Carbon 48, 452–455 (2010)CrossRefGoogle Scholar
  17. 17.
    M.R. Smith, E.W. Bittner, W. Shi, J.K. Johnson, B.C. Bockrath, J. Phys. Chem. B 107, 3752–3760 (2003)CrossRefGoogle Scholar
  18. 18.
    J.M. Blackman, J.W. Patrick, A. Arenillas, W. Shi, C.E. Snape, Carbon 44, 1376–1385 (2006)CrossRefGoogle Scholar
  19. 19.
    K. Xia, Q. Gao, C. Wu, S. Song, M. Ruan, Carbon 45, 1989–1996 (2007)CrossRefGoogle Scholar
  20. 20.
    R.T. Yang, Carbon 38, 623–626 (2000)CrossRefGoogle Scholar
  21. 21.
    D. Qu, Chem. Eur. J. 14, 1040–1046 (2008)CrossRefPubMedGoogle Scholar
  22. 22.
    H. Wang, Q. Gao, J. Hu., J. Am. Chem. Soc. 131, 7016–7022 (2009)CrossRefPubMedGoogle Scholar
  23. 23.
    D. Barrera, M. Dávila, V. Cornette, J.C. Alexandre de Oliveira, R.H. López, K. Sapag, Microporous Mesoporous Mater. 180, 71–78 (2013)CrossRefGoogle Scholar

Copyright information

© Springer Science+Business Media, LLC, part of Springer Nature 2017

Authors and Affiliations

  • Juliana M. Juárez
    • 1
  • Marcos Gómez Costa
    • 1
  • Oscar A. Anunziata
    • 1
    Email author
  1. 1.Centro de Investigación en Nanociencia y Nanotecnología (NANOTEC), Facultad Regional CórdobaUniversidad Tecnológica Nacional, Maestro López y Cruz Roja ArgentinaCórdobaArgentina

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