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Two directions of the reaction of 3,4-dihydroxy-6-oxoalka-2,4-dienoic acid esters with anthranilic acid hydrazide

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Abstract

Methyl 3,4-dihydroxy-6-oxoalka-2,4-dienoates reacted with anthranilic acid hydrazide to give methyl [5-alkyl-1-(2-aminobenzamido)-2-hydroxy-3-oxo-2,3-dihydro-1H-pyrrol-2-yl]acetates. The reaction of anthranilic acid hydrazide with ethyl 3,4-dihydroxy-6-oxohepta-2,4-dienoate afforded ethyl (2Z)-(3a-hydroxy-2-methyl-10-oxo-3,3a,5,10-tetrahydro-4H-pyrazolo[5,1-c][1,4]benzodiazepin-4-ylidene)acetate as solvate with one methanol molecule. The structure of the isolated compounds was determined on the basis of IR and NMR spectra and X-ray diffraction data.

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References

  1. Mukovoz, P.P. and Koz’minykh, V.O., Izv. Vyssh. Uchebn. Zaved., Povolzh. Region. Estestv. Nauki, 2013, vol. 2, no. 2, p. 91.

    Google Scholar 

  2. Mukovoz, P.P., Cand. Sci. (Chem.) Dissertation, Yaroslavl, 2010.

    Google Scholar 

  3. Mukovoz, P.P. and Koz’minykh, V.O., Vestn. Yuzhno- Ural. Gos. Univ., Ser. Khim., 2014, vol. 6, no. 3, p. 11.

    Google Scholar 

  4. Mukovoz, P.P., Tarasova, V.A., and Koz’minykh, V.O., Russ. J. Org. Chem., 2014, vol. 50, p. 1687.

    Article  CAS  Google Scholar 

  5. Pavlova, E.Yu., Cand. Sci. (Chem.) Dissertation, Perm, 1995.

    Google Scholar 

  6. Shurov, S.N., Pavlova, E.Yu., Livantsova, L.I., Zaitseva, G.S., and Andreichikov, Yu.S., Russ. J. Org. Chem., 1993, vol. 29, p. 1890.

    Google Scholar 

  7. Mukovoz, P.P., Andreeva, V.A., El’tsov, O.S., Koz’minykh, E.N., and Koz’minykh, V.O., Russ. J. Gen. Chem., 2015, vol. 85, p. 1386.

    Article  CAS  Google Scholar 

  8. Mukovoz, P.P., Koz’minykh, V.O., Andreeva, V.A., Koz’minykh, E.N., and El’tsov, O.S., Russ. J. Org. Chem., 2015, vol. 51, p. 1453.

    Article  CAS  Google Scholar 

  9. Mukovoz, P.P., Koz’minykh, V.O., and Dvorskaya, O.N., Bashk. Khim. Zh., 2010, vol. 17, no. 3, p. 23.

    CAS  Google Scholar 

  10. Mukovoz, P.P., Karmanova, O.G., Koz’minykh, E.N., and Koz’minykh, V.O., Bashk. Khim. Zh., 2012, vol. 19, no. 2, p. 12.

    CAS  Google Scholar 

  11. Sheldrick, G.M., Acta Crystallogr., Sect. A, 2008, vol. 64, p. 112.

    Article  CAS  Google Scholar 

Download references

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Authors and Affiliations

  1. Orenburg Branch, Moscow Technological Institute, pr. Pobedy 75, Orenburg, 460018, Russia

    P. P. Mukovoz

  2. Orenburg State University, pr. Pobedy 13, Orenburg, 460018, Russia

    A. V. Gorbunova

  3. Perm State Humanitarian Pedagogical University, Sibirskaya ul. 24, Perm, 614990, Russia

    V. O. Koz’minykh & E. N. Koz’minykh

  4. Postovskii Institute of Organic Synthesis, Ural Branch, Russian Academy of Sciences, ul. S. Kovalevskoi/Akademicheskaya 22/20, Yekaterinburg, 620990, Russia

    P. A. Slepukhin & I. N. Ganebnykh

  5. Yeltsin Ural Federal University, ul. Mira 19, Yekaterinburg, 620002, Russia

    P. A. Slepukhin, I. N. Ganebnykh & O. S. El’tsov

Authors
  1. P. P. Mukovoz
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  2. A. V. Gorbunova
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  3. V. O. Koz’minykh
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  4. P. A. Slepukhin
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  5. I. N. Ganebnykh
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  6. O. S. El’tsov
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  7. E. N. Koz’minykh
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Corresponding author

Correspondence to P. P. Mukovoz.

Additional information

Original Russian Text © P.P. Mukovoz, A.V. Gorbunova, V.O. Koz’minykh, P.A. Slepukhin, I.N. Ganebnykh, O.S. El’tsov, E.N. Koz’minykh, 2016, published in Zhurnal Organicheskoi Khimii, 2016, Vol. 52, No. 7, pp. 999–1005.

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Mukovoz, P.P., Gorbunova, A.V., Koz’minykh, V.O. et al. Two directions of the reaction of 3,4-dihydroxy-6-oxoalka-2,4-dienoic acid esters with anthranilic acid hydrazide. Russ J Org Chem 52, 993–999 (2016). https://doi.org/10.1134/S1070428016070125

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  • DOI: https://doi.org/10.1134/S1070428016070125

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