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Reaction of 3,4-dioxohexane-1,6-dioic acid esters with 2,4-dinitrophenylhydrazine

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Abstract

Reaction was studied of 3,4-dihydroxyhexa-2,4-diene-1,6-dioic acid esters with 2,4-dinitrophenylhydrazine that led to the formation of esters of (3E)-3-[2-(2,4-dinitrophenyl)-hydrazinylidene]-4-oxohexane-1,6-dioic and (3E,4E)-3,4-bis[2-(2,4-dinitrophenyl)hydrazinylidene]-hexane-1,6-dioic acids. The structural features of compounds synthesized were established from the data of IR and NMR spectra and X-ray diffraction (XRD) analysis.

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Authors and Affiliations

  1. Moscow Technologic Institute, Orenburg Branch, pr. Pobedy 75, Orenburg, 460018, Russia

    P. P. Mukovoz

  2. Perm State Humanitarian and Pedagogical University, Perm, Russia

    V. O. Koz’minykh & E. N. Koz’minykh

  3. Postovskii Institute of Organic Synthesis, Ural Branch, Russian Academy of Sciences, Yekaterinburg, Russia

    P. A. Slepukhin & I. N. Ganebnykh

  4. El’tsin Ural Federal University, Yekaterinburg, Russia

    P. A. Slepukhin, I. N. Ganebnykh & O. S. El’tsov

  5. Orenburg State University, Orenburg, Russia

    A. V. Gorbunova

Authors
  1. P. P. Mukovoz
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  2. V. O. Koz’minykh
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  3. P. A. Slepukhin
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  4. I. N. Ganebnykh
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  5. O. S. El’tsov
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  6. A. V. Gorbunova
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  7. E. N. Koz’minykh
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Corresponding author

Correspondence to P. P. Mukovoz.

Additional information

Original Russian Text © P.P. Mukovoz, V.O. Koz’minykh, P.A. Slepukhin, I.N. Ganebnykh, O.S. El’tsov, A.V. Gorbunova, E.N. Koz’minykh, 2016, published in Zhurnal Organicheskoi Khimii, 2016, Vol. 52, No. 5, pp. 652–658.

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Mukovoz, P.P., Koz’minykh, V.O., Slepukhin, P.A. et al. Reaction of 3,4-dioxohexane-1,6-dioic acid esters with 2,4-dinitrophenylhydrazine. Russ J Org Chem 52, 636–643 (2016). https://doi.org/10.1134/S1070428016050043

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  • DOI: https://doi.org/10.1134/S1070428016050043

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