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Synthesis of Spherical Copper Microparticles by Reduction of Cu(II) Ions with Benzyl Alcohol in the Presence of 2-[2-(2-Methoxyethoxy)etoxy]acetic Acid

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Abstract

Spherical copper microparticles were synthesized by reduction of Cu2+ ions with benzyl alcohol in the presence of 2-[2-(2-methoxyethoxy)ethoxy]acetic acid at 195°C. The resulting particles were characterized by X-ray phase analysis and electron microscopy. The influence of the synthesis conditions (synthesis temperature and time, as well as stabilizer, copper ions, and sodium hydroxide concentrations) on the size, morphology, and degree of polydispersity of the resulting copper particles was assessed.

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Funding

This study was carried out within the framework of the state assignment for the Institute of Solid State Chemistry and Mechanochemistry, Siberian Branch, Russian Academy of Sciences (project no. 0237-2019-0002).

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Authors and Affiliations

  1. Institute of Solid State Chemistry and Mechanochemistry, Siberian Branch, Russian Academy of Sciences, 630128, Novosibirsk, Russia

    O. A. Logutenko, A. I. Titkov & A. M. Vorobyov

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  1. O. A. Logutenko
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  2. A. I. Titkov
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  3. A. M. Vorobyov
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Correspondence to O. A. Logutenko.

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Logutenko, O.A., Titkov, A.I. & Vorobyov, A.M. Synthesis of Spherical Copper Microparticles by Reduction of Cu(II) Ions with Benzyl Alcohol in the Presence of 2-[2-(2-Methoxyethoxy)etoxy]acetic Acid. Russ J Gen Chem 90, 1489–1494 (2020). https://doi.org/10.1134/S1070363220080162

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