Skip to main content
Log in

Synthesis and thermal analysis of a Ni(II) complex of nicotinamide

  • Selected articles originally published in Russian in Rossiiskii Khimicheskii Zhurnal (Russian Chemistry Journal)
  • Published:
Russian Journal of General Chemistry Aims and scope Submit manuscript

Abstract

Nickel(II) bisnicotinamide sulfate was synthesized, isolated, and studied by means of FTIR spectroscopy, thermogravimetry, and differential scanning calorimetry with simultaneous mass-spectrometry analysis of pyrolysis products. The order the molecules are evolved from the coordination compound during thermal treatment is determined. The total heat effects of the processes involved in pyrolysis are estimated.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Similar content being viewed by others

References

  1. Fontecilla–Camp, J.C., Bioinorganic Chemistry. Structure and Bonding, Berlin: Springer, 1998, vol. 91, pp. 1–30.

    Google Scholar 

  2. Thauer, R.K., Diekert, G., and Schonheit, P., Trends Biochem. Sci., 1980, vol. 5, pp. 304–306.

    Article  CAS  Google Scholar 

  3. Yokoi, K., Uthus, E.O., Penland, J.G., and Nielsen, F.H., J. Trace Elem. Med. Biol., 2014, vol. 28, pp. 436–440.

    Article  CAS  Google Scholar 

  4. Haase, H., Hebel, S., Engelhardt, G., and Link, R., Metallomics, 2015, vol. 7, pp. 97–106.

    Article  Google Scholar 

  5. Thyssen, J.P., Linneberg, A., Menne, T., and Johansen, J.D., Contact Dermatitis, 2007, vol. 57, pp. 287–299.

    Article  Google Scholar 

  6. Kasprzak, K.S., Sunderman, F.W., and Salnikow, K., Mutation Res., 2003, vol. 533, pp. 67–97.

    Article  CAS  Google Scholar 

  7. Dunnick, J.K., Elwell, M.R., Radovsky, A.E., Benson, J.M., Hahn, F.F., Nikula, K.J., Barr, E.B., and Hobbs, C.H., Cancer Res., 1995, vol. 55, pp. 5251–5256.

    CAS  Google Scholar 

  8. Mashkovskii, M.D., Lekarstvennye sredstva (Drugs), Moscow Novaya Volna, 2005.

    Google Scholar 

  9. Vinogradov, V.V., Nekofermentnye funktsii vitamina PP(Noncoferment Functions of Vitamin PP), Minsk Nauka i Tekhnika, 1987.

    Google Scholar 

  10. Hino, T. and Ford, J.L., Int. J. Pharm., 2001, vol. 226, pp. 53–60.

    Article  CAS  Google Scholar 

  11. Lee, J., Lee, S.C., Acharya, G., Chang, C., and Park, K., Pharm. Res., 2003, vol. 20, no. 7, pp. 1022–1030.

    Article  CAS  Google Scholar 

  12. Lim, L.-Y., and Go, L.-M., Eur. J. Pharm. Sci., 2000, vol. 10, pp. 17–28.

    Article  CAS  Google Scholar 

  13. Evstigneev, M.P., Evstigneev, VP., Santiago, A.A.H., and Davis, D.B., Eur. J. Pharm. Sci., 2006, vol. 28, pp. 59–66.

    Article  CAS  Google Scholar 

  14. Hashmi, M., Assay of Vitamins in Pharmaceutical Preparations, London Wiley, 1973.

    Google Scholar 

  15. Hughes, M.N., The Inorganic Chemistry of Biological Processes, Chichester: Wiley, 1981, 2nd ed.

    Google Scholar 

  16. Al–Saif, F.A. and Refat, M.S., J. Mol. Struct., 2012, vol. 1021, pp. 40–52.

    Article  Google Scholar 

  17. Arias, C.A. and Murray, B.E., N. Engl. J. Med., 2009, vol. 360, pp. 439–443.

    Article  CAS  Google Scholar 

  18. Gamov, G.A., Dushina, S.V, Sharnin, V.A., and Zavalishin, M.N., Centr. Eur. J. Chem., 2013, vol. 11, no. 12, pp. 1959–1963.

    CAS  Google Scholar 

  19. Gamov, G.A., Dushina, S.V., and Sharnin, V.A., Russ. J. Phys. Chem. A, 2014, vol. 88, no. 5, pp. 779. doi 10.1134/S0036024414050094

    Google Scholar 

  20. Gamov, G.A., Grazhdan, K.V, Dushina, S.V, and Sharnin, V.A., J. Chem. Thermodyn., 2015, vol. 82, pp. 116–124.

    Article  Google Scholar 

  21. Kose, D.A. and Necefoglu, H., J. Therm. Anal. Cal., 2008, vol. 93, pp. 509–514.

    Article  Google Scholar 

  22. Tsierkezos, N.S. and Molinou, I.E., J. Chem. Eng. Data, 2000, vol. 45, pp. 819–822.

    Article  CAS  Google Scholar 

  23. Tsierkezos, N.S. and Molinou, I.E., J. Chem. Eng. Data, 2001, vol. 46, pp. 1399–1403.

    Article  Google Scholar 

  24. Bruno, T.J. and Svoronos, P.D.N., Handbook of Basic Tables for Chemical Analysis, Boca Raton: CRC, 2011, 3rd ed.

    Google Scholar 

  25. Brown, D. W., Floyd, A. J., and Sainsbury, M., Organic Spectroscopy, Chichester Wiley, 1988.

    Google Scholar 

  26. Eisenberg, D. and Kauzmann, W., The Structure and Properties of Water, New York Oxford Univ., 1969.

    Google Scholar 

  27. Paul, R.C., Sreenathan, B.R., and Chadha, S.L., J. Inorg. Nucl. Chem., 1966, vol. 28, no. 5, pp. 1225–1235.

    Article  CAS  Google Scholar 

  28. Paul, R.C. and Chadha, S.L., J. Inorg. Nucl. Chem., 1969, vol. 31, no. 9, pp. 2753–2757.

    Article  CAS  Google Scholar 

  29. Nakamoto, K., Infrared and Raman Spectra of Inorganic and Coordination Compounds, New York: Wiley. 1986, 4th ed., pp. 139–248.

  30. Adler, H.H. and Kerr, P.F., Am. Mineral., 1965, vol. 50, pp. 132–147.

    CAS  Google Scholar 

  31. Efthymiou, C.G., Kitos, A.A., Raptopoulou, C.P., Perlepes, S.P., Escuer, A., and Papatriantafyllopoulou, C., Polyhedron, 2009, vol. 28, pp. 3177–3184.

    Article  CAS  Google Scholar 

  32. Maneva, M., Rizova, D., Genov, L., and Liptay, G., J. Therm. Anal., 1990, vol. 36, pp. 915–922.

    Article  CAS  Google Scholar 

  33. Winkler, J.K., Karow, W., and Rademacher, P., Arch. Org. Chem., 2000, no. 4, pp. 576–602.

    Google Scholar 

  34. Minkin, V.I., Simkin, B.Ya., and Minyaev, R.M., Teoriya stroeniya molekul (Theory of Molecular Structure), Rostov-on-Don Feniks, 1997.

    Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to G. A. Gamov.

Additional information

Original Russian Text © G.A. Gamov, M.N. Zavalishin, S.V. Dushina, V.A. Sharnin, 2015, published in Rossiiskii Khimicheskii Zhurnal, 2015, Vol. 59, Nos. 1–2, pp. 68–73.

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Gamov, G.A., Zavalishin, M.N., Dushina, S.V. et al. Synthesis and thermal analysis of a Ni(II) complex of nicotinamide. Russ J Gen Chem 87, 613–618 (2017). https://doi.org/10.1134/S1070363217030380

Download citation

  • Received:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1134/S1070363217030380

Navigation