Skip to main content
SpringerLink
Log in

Vanadium(III) dithiophosphate complex [V(S2P(O-iso-Pr)2)3]: synthesis and structure

  • Published:
Russian Journal of Coordination Chemistry Aims and scope Submit manuscript

Abstract

The reaction of [VO(OPr)3] with (iso-PrO)2P(S)SH (Pr is n-propyl, and iso-Pr is isopropyl) followed by the treatment with hexamethyldisilthiane (Me3SiSSiMe3) affords the vanadium(III) dithiophosphate complex [V(S2P(O-iso-Pr)2)3]. The structure of the complex is determined by X-ray diffraction analysis (CIF file CCDC 986354).

This is a preview of subscription content, log in via an institution to check access.

Access this article

Log in via an institution

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Institutional subscriptions

Similar content being viewed by others

References

  1. Simonnet-Jegat, C., Secheresse, F., Chem. Rev., 2003, vol. 101, p. 2601.

    Article  Google Scholar 

  2. Sokolov, M.N. and Fedin, V.P., Coord. Chem. Rev., 2004, vol. 248, p. 925.

    Article  CAS  Google Scholar 

  3. Sendlinger, S.C., Nicholson, J.R., Lobkovsky, E.B., et al., Inorg. Chem., 1993, vol. 32, p. 204.

    Article  CAS  Google Scholar 

  4. Duraj, S.A., Andras, M.T., and Kibala, P.A., Inorg. Chem., 1990, vol. 29, p. 1232.

    Article  CAS  Google Scholar 

  5. Halbert, T.R., Hutchings, L.L., Rhodes, R., et al., J. Am. Chem. Soc., 1986, vol. 108, p. 6437.

    Article  CAS  Google Scholar 

  6. Money, J.K., Huffman, J.C., and Christou, G., Inorg. Chem., 1988, vol. 27, p. 507.

    Article  CAS  Google Scholar 

  7. Tiekink, E.R.T., Yan, X.F., and Young, C.G., Aust. J. Chem., 1992, vol. 45, p. 897.

    Article  CAS  Google Scholar 

  8. Yang, Y., Huang, L., Liu, Q., et al., Acta Crystallogr., Sect. C: Cryst. Struct. Commun., 1991, vol. 47, p. 2085.

    Article  Google Scholar 

  9. Sokolov, M.N., Virovets, A.V., Oekler, O., et al., Inorg. Chim. Acta, 2002, vol. 331, p. 25.

    Article  CAS  Google Scholar 

  10. Sheldrick, G.M., SADABS. Program for Empirical X-Ray Absorption Correction, Bruker AXS, 1990–2007.

    Google Scholar 

  11. Sheldrick, G.M., SHELXTL. Programs for Structure Solution and Refinement, Bruker AXS, 1990–2007.

    Google Scholar 

  12. Furlani, C., Tomlinson, A.G., Porta, P., and Sgamelotti, A., J. Chem. Soc. A, 1970, p. 2929.

    Google Scholar 

  13. Blatov, V.A., Newsletter Commission on Crystallographic Computing of International Union of Crystallography, 2006, no. 7, p. 4.

    Google Scholar 

  14. Kepert, D.L., Inoganic Stereochemistry, Berlin: Springer, 1982.

    Book  Google Scholar 

  15. Schousboe-Jensen, H.V.F. and Hazell, R.G., Acta Chem. Scand., 1972, vol. 26, p. 1375.

    Article  CAS  Google Scholar 

Download references

Author information

Authors and Affiliations

  1. Nikolaev Institute of Inorganic Chemistry, Siberian Branch, Russian Academy of Sciences, pr. akademika Lavrent’eva 3, Novosibirsk, 630090, Russia

    A. V. Rogachev, A. V. Virovets & M. N. Sokolov

  2. Novosibirsk State University, ul. Pirogova 2, Novosibirsk, 630090, Russia

    M. N. Sokolov

Authors
  1. A. V. Rogachev
    View author publications

    You can also search for this author in PubMed Google Scholar

  2. A. V. Virovets
    View author publications

    You can also search for this author in PubMed Google Scholar

  3. M. N. Sokolov
    View author publications

    You can also search for this author in PubMed Google Scholar

Corresponding author

Correspondence to M. N. Sokolov.

Additional information

Original Russian Text © A.V. Rogachev, A.V. Virovets, M.N. Sokolov, 2014, published in Koordinatsionnaya Khimiya, 2014, Vol. 40, No. 10, pp. 604–607.

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Rogachev, A.V., Virovets, A.V. & Sokolov, M.N. Vanadium(III) dithiophosphate complex [V(S2P(O-iso-Pr)2)3]: synthesis and structure. Russ J Coord Chem 40, 722–725 (2014). https://doi.org/10.1134/S1070328414100091

Download citation

  • Received:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1134/S1070328414100091

Keywords

Search

Navigation