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The Effect of the Mode of Heat Treatment and Mechanoactivation of Kaolinite on Mullite Formation

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Abstract

The effect of the rate of heating of kaolinite Al4[Si4O10](OH)8 on its transformation into mullite 3Al2O3 · 2SiO2 has been studied. The mullite yield increases with the heating rate. The temperature rise at a high rate promotes rapid dehydration of kaolinite, which is accompanied by detachment of hydroxo groups and structural disordering. The effects of preliminary mechanoactivation of kaolin in a ball-and-ring mill, which abrases a material, and in a planetary mill, in which shock loads dominate, have been compared. It has been established that attrition treatment is ineffective. The intense impact-abrasion treatment in a planetary mill breaks up packets and layers; a part of hydroxo groups appear on the outer surface of polycrystallites, which facilitates dehydroxylation.

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ACKNOWLEDGMENTS

This study was carried out using the resources of the Center for Collective Use of Ivanovo State University of Chemistry and Technology.

Funding

This study was supported by the Ministry of Science and Higher Education of the Russian Federation, project no. 075-15-2021-671.

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Authors and Affiliations

  1. Ivanovo State University of Chemistry and Technology, 153000, Ivanovo, Russia

    N. V. Filatova, N. F. Kosenko & M. A. Badanov

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  1. N. V. Filatova
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  2. N. F. Kosenko
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  3. M. A. Badanov
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Correspondence to N. V. Filatova.

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The authors declare that they have no conflicts of interest.

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Translated by E. Bondareva

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Filatova, N.V., Kosenko, N.F. & Badanov, M.A. The Effect of the Mode of Heat Treatment and Mechanoactivation of Kaolinite on Mullite Formation. Tech. Phys. Lett. 49, 81–85 (2023). https://doi.org/10.1134/S1063785023700025

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  • DOI: https://doi.org/10.1134/S1063785023700025

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