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Crystal structures of two organic salts of 1,2,3,4-tetrahydro-1,10-phenanthroline

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Abstract

Two organic salts of 1,2,3,4-tetrahydro-1,10-phenanthroline (tphen), namely (oaH)(tphenH) (1) and (ssa)(tphenH)·H2O (2) (oaH2 is oxalic acid, ssaH is 5-sulfosalicylic acid), were synthesized and structurally characterized. Both compounds contain tphenH+ cations but illustrate different crystal structures. The tphenH+ cations show a cross-stacking packing model in 1 but display a herringbone packing model in 2.

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References

  1. F. Li, Y. Mulyana, M. Feterl, J. M. Warner, J. G. Collins, and F. R. Keene, Dalton. Trans. 40, 5032 (2011).

    Article  Google Scholar 

  2. S. P. Chen, Y. Guo, Q. L. Chen, M. Li, L. J. Yuan, and J. T. Sun, J. Coord. Chem. 61, 973 (2008).

    Article  Google Scholar 

  3. N. Raman and J. Joseph, Russ. J. Inorg. Chem. 55, 1064 (2010).

    Article  Google Scholar 

  4. M. Li, J. F. Xiang, S. M. Wu, S. P. Chen, L. J. Yuan, H. Li, H. J. He, and J. T. Sun, J. Mol. Struct. 840, 119 (2007).

    Article  ADS  Google Scholar 

  5. Q. Y. Chen, H. J. Fu, W. H. Zhu, Y. Qi, Z. P. Ma, K. D. Zhao, and J. Gao, Dalton Trans. 40, 4414 (2011).

    Article  Google Scholar 

  6. F. Y. Yi, Q. P. Lin, T. H. Zhou, and J. G. Mao, Cryst. Growth Des. 10, 1788 (2010).

    Article  Google Scholar 

  7. M. A. Rizvi, N. Teshima, and G. M. Peerzada, Croat. Chem. Acta 86, 345 (2013).

    Article  Google Scholar 

  8. V. Lippolis and M. Shamsipur, J. Indian Chem. Soc. 3, 105 (2006).

    Google Scholar 

  9. N. Shan, A. D. Bond, and W. Jones, New J. Chem. 27, 365 (2003).

    Article  Google Scholar 

  10. C. V. K. Sharma and A. Clearfield, J. Am. Chem. Soc. 122, 4394 (2000).

    Article  Google Scholar 

  11. S. M. Wu, S. P. Chen, M. Li, J. F. Xiang, Y. Xiao, and L. J. Yuan, Cryst. Eng. Commun. 9, 907 (2007).

    Article  Google Scholar 

  12. C. Metallinos, F. B. Barrett, J. L. Chaytor, and M. E. A. Heska, Org. Lett. 6, 3641 (2004).

    Article  Google Scholar 

  13. I. Eckhard, R. Fielden, and L. Summers, Aust. J. Chem. 28, 1149 (1975).

    Article  Google Scholar 

  14. P. C. Keller, R. L. Marks, and J. V. Rund, Polyhedron 2, 595 (1983).

    Article  Google Scholar 

  15. B. C. Ranu, U. Jana, and A. Sarkar, Synth. Commun. 28, 485 (1998).

    Article  Google Scholar 

  16. A. Srikrishna, T. Jagadeeswar Reddy, and R. Viswajanani, Tetrahedron 52, 1631 (1996).

    Article  Google Scholar 

  17. C. Bianchini, V. Dal Santo, A. Meli, S. Moneti, R. Psaro, L. Sordelli, and F. Vizza, Inorg. Chim. Acta 361, 3677 (2008).

    Article  Google Scholar 

  18. S. P. Chen, P. Deng, C. F. Yuan, and L. J. Yuan, Cryst. Eng. Commun. 15, 1414 (2013).

    Article  Google Scholar 

  19. J. Deng, H. P. Su, and S. P. Chen, Crystallogr. Rep. 59, 1051 (2014).

    Article  ADS  Google Scholar 

  20. G. M. Sheldrick, Acta. Crystallogr. A 64, 112 (2008).

    Article  ADS  Google Scholar 

  21. C. F. Macrae, P. R. Edgington, P. McCabe, E. Pidcock, G. P. Shields, R. Taylor, M. Towler, and J. van de Streek, J. Appl. Crystallogr. 39, 453 (2006).

    Article  Google Scholar 

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Authors and Affiliations

  1. College of Chemical and Environmental Engineering, Hubei University for Nationalities, Enshi, 445000, P. R. China

    Y. Zheng

  2. College of Materials Science and Engineering, Guilin University of Technology, Guilin, 541004, P. R. China

    H. P. Yi, B. H. Song & S. P. Chen

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  1. Y. Zheng
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  2. H. P. Yi
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  3. B. H. Song
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  4. S. P. Chen
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Corresponding author

Correspondence to S. P. Chen.

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The article is published in the original.

These two authors contributed equally to this work.

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Zheng, Y., Yi, H.P., Song, B.H. et al. Crystal structures of two organic salts of 1,2,3,4-tetrahydro-1,10-phenanthroline. Crystallogr. Rep. 61, 1090–1095 (2016). https://doi.org/10.1134/S1063774516070154

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  • DOI: https://doi.org/10.1134/S1063774516070154

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