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Layered-Fibrous Composite with a Niobium-Based Matrix Reinforced with Single-Crystal Sapphire Fibers

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Abstract

In this paper, we obtain samples of composite materials with a layered niobium-based matrix unidirectionally reinforced with single-crystal sapphire fibers using the solid-phase method of diffusion welding. Sapphire fibers are obtained by the Stepanov method (EFG). As a result of tests, the dependences of the strength of such fibers on the length are obtained for the first time. The strength values ​​correspond to the global level. X-ray spectral microanalysis of the obtained materials is performed. The formation of solid solutions and intermetallic compounds of the Nb-Al system during composite-structure formation is established. Strength tests (500–700 MPa) are carried out and the effective surface energy of fracture of the composites is determined ((9–49) × 103 J/m2), and their correlation with the fabrication modes is established. The features of the fracture structure of such materials and the processes inhibiting its fracturing under load are studied.

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ACKNOWLEDGEMENTS

We are grateful to D.O. Stryukov, D.G. Pizhenin, S.L. Shikunov, I.S. Zheltyakova, and A.N. Nekrasov for their help in experimental research.

Funding

This work was supported by the Institute of Solid State Physics, Russian Academy of Sciences, within the framework of the State Assignment and in part by the Russian Foundation for Basic Research, project no. 20-03-00296.

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Correspondence to V. M. Kiiko, V. P. Korzhov, V. N. Kurlov or K. A. Khvostunkov.

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Translated by A. Ivanov

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Kiiko, V.M., Korzhov, V.P., Kurlov, V.N. et al. Layered-Fibrous Composite with a Niobium-Based Matrix Reinforced with Single-Crystal Sapphire Fibers. J. Surf. Investig. 14, 1126–1132 (2020). https://doi.org/10.1134/S1027451020060075

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