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Sodium Chromium Arsenate Phosphates: Preparation, Structure, and Thermal Properties

  • SYNTHESIS AND PROPERTIES OF INORGANIC COMPOUNDS
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Abstract

Arsenate phosphates \({\text{N}}{{{\text{a}}}_{3}}{\text{C}}{{{\text{r}}}_{2}}{{({\text{As}}{{{\text{O}}}_{4}})}_{x}}{{({\text{P}}{{{\text{O}}}_{4}})}_{{3\,\, - \,\,x}}}\) (1.75 ≤ x ≤ 3.0) were prepared by coprecipitation. Their unit cell parameter was a linear function of composition: a (Å) = 0.0967x + 11.873. The Na3Cr2(AsO4)2PO4 crystal structure was refined by the Rietveld method; the coordinates of basal atoms and bond lengths were calculated. A garnet solid solution crystallizes at 600–650°C; transition to a high−temperature rhombohedral structure occurred at 994–1044°C. The thermal expansion of the low-temperature phase having a garnet structure was studied in the range from –130 to 200°C. The solid solution samples expanded isotropically and had small thermal expansion.

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Funding

The study was supported by the Russian Science Foundation (project no. 23-23-00044), https://rscf.ru/project/23-23-00044/.

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Authors and Affiliations

  1. Nizhny Novgorod State University, 603950, Nizhny Novgorod, Russia

    E. A. Pyaterikov, V. I. Pet’kov & D. G. Fukina

  2. Kola Scientific Center, Russian Academy of Sciences, 184209, Apatity, Russia

    E. Yu. Borovikova

Authors
  1. E. A. Pyaterikov
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  2. V. I. Pet’kov
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  3. D. G. Fukina
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  4. E. Yu. Borovikova
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Correspondence to E. A. Pyaterikov.

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Translated by O. Fedorova

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Pyaterikov, E.A., Pet’kov, V.I., Fukina, D.G. et al. Sodium Chromium Arsenate Phosphates: Preparation, Structure, and Thermal Properties. Russ. J. Inorg. Chem. 68, 1371–1379 (2023). https://doi.org/10.1134/S0036023623601927

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  • DOI: https://doi.org/10.1134/S0036023623601927

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