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Water Forms on the Surface and in the Bulk of Silicon Dioxide

  • PHYSICOCHEMICAL ANALYSIS OF INORGANIC SYSTEMS
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Abstract

Thermodynamic characteristics and water evaporation mechanism from silica structure in temperature range 100–1000°С have been studied by thermogravimetry, mass spectrometry, 1Н and 29Si NMR. It has been shown that liquid, surface-bound, and molecular-dispersed water is present on the surface and in the bulk of silica particles. The role of different (ОН)n groups in the structural change of silica upon thermal and thermal steam treatment has been shown. A method for preparation of anhydrous silica used in the manufacture of high-quality quartz glass has been proposed.

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ACKNOWLEDGMENTS

This work was performed under the State Assignment in the field of basic research for the Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences.

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Authors and Affiliations

  1. Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences, 119991, Moscow, Russia

    G. P. Panasyuk, I. V. Kozerozhets, I. L. Voroshilov & V. I. Privalov

  2. Moscow State University, 119991, Moscow, Russia

    Yu. D. Ivakin & M. N. Danchevskaya

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  1. G. P. Panasyuk
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  2. I. V. Kozerozhets
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  3. I. L. Voroshilov
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  4. Yu. D. Ivakin
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  6. M. N. Danchevskaya
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Correspondence to I. V. Kozerozhets.

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Translated by I. Kudryavtsev

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Panasyuk, G.P., Kozerozhets, I.V., Voroshilov, I.L. et al. Water Forms on the Surface and in the Bulk of Silicon Dioxide. Russ. J. Inorg. Chem. 66, 724–730 (2021). https://doi.org/10.1134/S0036023621050120

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