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Crystallization in the Bi2O3-Fe2O3-NaOH system upon microwave-assisted hydrothermal synthesis

  • Synthesis and Properties of Inorganic Compounds
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Abstract

Crystallization processes in the Bi2O3-Fe2O3-NaOH system upon microwave-assisted hydrothermal synthesis have been studied to reveal the effect of the mineralizer concentration, temperature, degree of filling of the autoclave, and the preparation of precursors on the phase composition and the morphology of the reaction product. Submicron powders of bismuth ferrite Bi2Fe4O9 have been synthesized.

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Authors and Affiliations

  1. Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Science, Leninskii pr. 31, Moscow, 119991, Russia

    A. V. Egorysheva, O. M. Gaitko, P. O. Rudnev, T. B. Kuvshinova & A. D. Yapryntsev

Authors
  1. A. V. Egorysheva
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  2. O. M. Gaitko
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  3. P. O. Rudnev
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  4. T. B. Kuvshinova
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  5. A. D. Yapryntsev
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Correspondence to A. V. Egorysheva.

Additional information

Original Russian Text © A.V. Egorysheva, O.M. Gaitko, P.O. Rudnev, T.B. Kuvshinova, A.D. Yapryntsev, 2015, published in Zhurnal Neorganicheskoi Khimii, 2015, Vol. 60, No. 11, pp. 1425–1431.

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Egorysheva, A.V., Gaitko, O.M., Rudnev, P.O. et al. Crystallization in the Bi2O3-Fe2O3-NaOH system upon microwave-assisted hydrothermal synthesis. Russ. J. Inorg. Chem. 60, 1304–1310 (2015). https://doi.org/10.1134/S0036023615110042

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  • DOI: https://doi.org/10.1134/S0036023615110042

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