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Molecular and Crystal Structure of a Novel Mannich Quaternary Salt: 3-(Dimethylamino)-1-p-Tolylpropan-1-One Hydrochloride

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Abstract

A novel Mannich base is synthesized by the condensation of 4-methylacetophenone and dimethylamine hydrochloride in the presence of formaldehyde. The molecular and crystal structure of the title compound is confirmed by 1H, 13C NMR and IR spectroscopy, and single crystal X-ray diffraction.

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Authors and Affiliations

  1. Department of Chemistry, Rhodes University, Grahamstown, South Africa

    A. O. Ayeni & G. M. Watkins

  2. Department of Chemistry, Obafemi Awolowo University, Ile Ife, Nigeria

    A. O. Ayeni

  3. Department of Chemistry, Nelson Mandela Metropolitan University, Port Elizabeth, South Africa

    E. C. Hosten

Authors
  1. A. O. Ayeni
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  2. G. M. Watkins
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  3. E. C. Hosten
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Corresponding author

Correspondence to A. O. Ayeni.

Additional information

Original Russian Text © 2018 A. O. Ayeni, G. M. Watkins, E. C. Hosten.

The text was submitted by the authors in English. Zhurnal Strukturnoi Khimii, Vol. 59, No. 7, pp. 1746–1748, September-October, 2018.

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Ayeni, A.O., Watkins, G.M. & Hosten, E.C. Molecular and Crystal Structure of a Novel Mannich Quaternary Salt: 3-(Dimethylamino)-1-p-Tolylpropan-1-One Hydrochloride. J Struct Chem 59, 1688–1690 (2018). https://doi.org/10.1134/S0022476618070247

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  • DOI: https://doi.org/10.1134/S0022476618070247

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