Abstract
Additive manufacturing of ceramic materials has been evolving greatly. Yet, in the last 5 years, techniques based on lithography began to emerge with an emphasis on obtaining dense parts. The present work deals with the experimental study of additive manufacturing of 3Y zirconia via digital imaging projection. For this purpose, a commercial light projection system was set up with a mechanical spreader (blade) of paste layers on an x–y–z built platform. Formulations developed for a ceramic powder loaded with a photo-polymerizable resin and solvents were printed. After printing, the specimens were fired for solvents and resin removal, sintered and characterized. Digital projection (without filter) provided UV and visible light enough to polymerize the resin in layers of up to 50 µm thickness. Low-porosity zirconia bodies (3.4%) were obtained using mixtures with ceramic powder/resin concentration up to 50 vol%. Solvent removal under air pressure (3 bar) in an autoclave at 50 °C resulted in low lamination effects and avoided bubbles evolution. Three-point flexural test in non-machined sintered bars reached an average stress of 337 MPa. The results are very promising and demonstrate that the additive manufacturing of ceramic parts based on a digital imaging projection process is a viable alternative.
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References
Schwentenwein M, Homa J (2015) Additive manufacturing of dense alumina ceramics. Int J Appl Ceram Technol 12(1):1–7
Bose S, Vahabzadeh S, Bandyopadhyay A (2013) Bone tissue engineering using 3D printing. Mater Today 16(12):496–504
Ngo TD, Kashani A, Imbalzano G, Nguyen KTQ, Hui D (2018) Additive manufacturing (3D printing): a review of materials, methods, applications and challenges. Compos Part B-Eng 143:172–196
Varghese G, Moral M, Castro-Garcia M, Lopez-Lopez JJ, Marin-Rueda JR, Yague-Alcaraz V, Hernandez-Afonso L, Ruiz-Morales JC, Canales-Vazquez J (2018) Fabrication and characterisation of ceramics via low-cost DLP 3D printing. Boletín De La Sociedad Española De Cerámica Y Vidrio 57(1):9–18
Ludwig T, von Seckendorff J, Troll C, Fischer R, Tonigold M, Rieger B, Hinrichsen O (2018) Additive manufacturing of Al2O3-based carriers for heterogeneous catalysis. Chem Ing Tech 90(5):703–707
Monzon M, Ortega Z, Hernandez A, Paz R, Ortega F (2017) Anisotropy of photopolymer parts made by digital light processing. Materials 10(1):64
Zocca A, Colombo P, Gomes CM, Gunster J (2015) Additive manufacturing of ceramics: issues, potentialities, and opportunities. J Am Ceram Soc 98(7):1983–2001
Muskin J, Ragusa M, Gelsthorpe T (2010) Three-dimensional printing using a photoinitiated polymer. J Chem Educ 87(5):512–514
Wang JC, Dommati H, Hsieh SJ (2019) Review of additive manufacturing methods for high-performance ceramic materials. Int J Adv Manuf Technol 103(5–8):2627–2647
Zhou C, Chen Y (2012) Additive manufacturing based on optimized mask video projection for improved accuracy and resolution. J Manuf Process 14(2):107–118
Bonada J, Muguruza A, Fernandez-Francos X, Ramis X (2018) Optimisation procedure for additive manufacturing processes based on mask image projection to improve Z accuracy and resolution. J Manuf Process 31:689–702
Bae CJ, Ramachandran A, Chung K, Park S (2017) Ceramic stereolithography: additive manufacturing for 3D complex ceramic structures. J Korean Ceram Soc 54(6):470–477
Nomoto R (1997) Effect of light wavelength on polymerization of light-cured resins. Dent Mater J 16(1):60–73
Chartier T, Dupas C, Geffroy PM, Pateloup V, Colas M, Cornette J et al (2017) Influence of irradiation parameters on the polymerization of ceramic reactive suspensions for stereolithography. J Eur Ceram Soc 37(15):4431–4436
Gentry SP, Halloran JW (2015) Light scattering in absorbing ceramic suspensions: effect on the width and depth of photopolymerized features. J Eur Ceram Soc 35(6):1895–1904
Ligon SC, Liska R, Stampfl J, Gurr M, Mulhaupt R (2017) Polymers for 3D printing and customized additive manufacturing. Chem Rev 117(15):10212–10290
Wang J-C, Dommati H (2018) Fabrication of zirconia ceramic parts by using solvent-based slurry stereolithography and sintering. Int J Adv Manuf Technol 98(5–8):1537–1546
Halloran JW (2016) Ceramic stereolithography: additive manufacturing for ceramics by photopolymerization. Annu Rev Mater Res 46(46):19–40
Badev A, Abouliatim Y, Chartier T, Lecamp L, Lebaudy P, Chaput C, Delage C (2011) Photopolymerization kinetics of a polyether acrylate in the presence of ceramic fillers used in stereolithography. J Photochem Photobiol Chem 222(1):117–122
Dumene R, Earle G, Williams C (2018) Characterization of additively manufactured cellular alumina dielectric structures. IEEE Trans Dielectr Electr Insul 25(6):2236–2240
Bourell D, Kruth JP, Leu M, Levy G, Rosen D, Beese AM et al (2017) Materials for additive manufacturing. CIRP Ann Manuf Technol 66(2):659–681
Layani M, Wang XF, Magdassi S (2018) Novel materials for 3D printing by photopolymerization. Adv Mater 30(41):1706344
Diptanshu, Young E, Ma C, Obeidat S, Pang B, Kang N (eds). (2018) Ceramic additive manufacturing using vat photopolymerization. In: ASME 2018 13th international manufacturing science and engineering conference, MSEC 2018
Wang XF, Schmidt F, Hanaor D, Kamm PH, Li S, Gurlo A (2019) Additive manufacturing of ceramics from preceramic polymers: a versatile stereolithographic approach assisted by thiol-ene click chemistry. Addit Manuf 27:80–90
Mistler RE, Twiname ER (2000) Tape casting: theory and practice. American Ceramic Society, Westerville
Nesaraj AS, Raj IA, Pattabiraman R (2002) Preparation of zirconia thin films by tape casting technique as electrolyte material for solid oxide fuel cells. Indian J Eng Mater Sci 9(1):58–64
Li KH, Zhao Z (2017) The effect of the surfactants on the formulation of UV-curable SLA alumina suspension. Ceram Int 43(6):4761–4767
Acknowledgements
This study was financed in part by the Superior Level Personnel Advancement Coordination (Coordenação de Aperfeiçoamento de Pessoal de Nível Superior ‘CAPES’) – Brasil - Finance Code 001 and FAPESP, Grant #2016/23910-0.
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do Amaral, L.B., Paschoa, J.L.F., Magalhães, D.V. et al. Preliminary studies on additive manufacturing of over 95% dense 3Y zirconia parts via digital imaging projection. J Braz. Soc. Mech. Sci. Eng. 42, 75 (2020). https://doi.org/10.1007/s40430-019-2157-1
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DOI: https://doi.org/10.1007/s40430-019-2157-1