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Effect of Bore Fluid Conditions on Structures and Properties of Poly(m-phenylene isophthalamide) Hollow Fiber Membranes

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Abstract

This study investigates the effects of bore fluid composition on the morphological characterization, mechanical properties, and membrane performance of poly(m-phenylene isophthalamide) (PMIA) hollow fiber membranes prepared by a dry-jet wet spinning method using a non-solvent induced phase separation (NIPS), as an attempt to manufacture and apply high-performance membranes. Scanning electron microscopy (SEM) analysis reveals that the addition of DMAc (or NMP) to the internal coagulant (bore fluid) based on deionized water induces a transition from finger-like to sponge-like pore structures in the final PMIA membranes. Mechanical properties analysis shows an increase in tensile strength and a decrease in elongation at break as the additive content in the bore fluid increases. Water permeability and rejection analysis present a trade-off trends, with higher additive content leading to reduced water permeability and increased rejection. In other words, despite the consistent changes observed in pore structure with changes in additive type and content in the bore fluid, achieving an optimal balance between high water permeability and low rejection remains a challenge through these structural control and changes. Therefore, for the development and application of high-performance PMIA-based hollow fiber membranes, it is necessary to control and optimize the pore structure of the final PMIA membrane through extensive research on various process parameters.

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The datasets used and/or analyzed during the current study are available from the corresponding author on reasonable request.

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Acknowledgements

This research was supported by a research Grant from the Ministry of Trade, Industry and Energy (MOTIE, Project No. 20010447), and we gratefully acknowledge for the support.

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Authors and Affiliations

  1. Department of Advanced Organic Materials and Textile System Engineering, Chungnam National University, Daejeon, 34134, Korea

    Hyeon-Woo Baek, Da Won Kim & Doo Hyun Baik

  2. Metrology and Measurement Division, Korean Agency for Technology and Standards (KATS), Ministry of Trade, Industry and Energy (MOTIE), Eumseong, 27737, Korea

    Min Ho Jee

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  1. Hyeon-Woo Baek
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  2. Da Won Kim
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Correspondence to Min Ho Jee or Doo Hyun Baik.

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Baek, HW., Kim, D.W., Jee, M.H. et al. Effect of Bore Fluid Conditions on Structures and Properties of Poly(m-phenylene isophthalamide) Hollow Fiber Membranes. Fibers Polym 24, 3457–3465 (2023). https://doi.org/10.1007/s12221-023-00325-2

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