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Contribution of sodium dodecyl sulphate and sodium lauric acid in the one-pot synthesis of intercalated ZnAl-layered double hydroxides

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Abstract

Anion surfactants, sodium dodecyl sulphate (SDS) and sodium lauric acid (SLA), with almost the same chain length but different anion groups were used together as intercalates to prepare intercalated ZnAl–layered double hydroxides (ZnAl–LDHs). Their composition, structure and morphology were characterized by Fourier transform infrared, X-ray fluorescence, thermogravimetric and X-ray diffraction (XRD). The results indicated SDS intended to maintain the lamellae structure of LDHs, but SLA was more likely to expand the basal spacings of LDHs in the present system. The arrangement of the surfactants in the interlayer of ZnAl–LDHs was also simulated by Materials Studio. The basal spacings of the LDHs calculated based on simulated structure consisted with that from XRD.

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Acknowledgement

This study was financially supported by the Fundamental Research Funds for the Central Universities (2-9-2013-49), National Key Laboratory of Minerals (09B003), China.

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Authors and Affiliations

  1. State Key Laboratory of Geological Processes & Mineral Resources, National Laboratory of Mineral Materials, School of Materials Science and Technology, China University of Geosciences, Beijing, 100083, China

    FENGZHU LV, ZILIN MENG, PENGGANG LI, YIHE ZHANG, GUOCHENG LV, QIAN ZHANG & ZHILEI ZHANG

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  1. FENGZHU LV
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  2. ZILIN MENG
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Correspondence to FENGZHU LV.

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LV, F., MENG, Z., LI, P. et al. Contribution of sodium dodecyl sulphate and sodium lauric acid in the one-pot synthesis of intercalated ZnAl-layered double hydroxides. Bull Mater Sci 38, 1079–1085 (2015). https://doi.org/10.1007/s12034-015-0956-2

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  • DOI: https://doi.org/10.1007/s12034-015-0956-2

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