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Nanocrystalline Ni25Co20Cu10Fe25Mn20 High-Entropy Alloys Prepared by Mechanical Alloying

  • Phase Transformation and Microstructure Evolution during Thermomechanical Processing
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Abstract

An Ni25Co20Cu10Fe25Mn20 high-entropy alloy (HEA) was produced using mechanical alloying. Similar to equiatomic NiCoCuFeMn alloy, a face-centered cubic single-phase nanocrystalline HEA was obtained after 28-h milling. The lattice parameter of this new HEA (0.360 nm) was slightly smaller than that of equiatomic alloy (0.361 nm). The crystallite size of the final product was ~ 9 nm, significantly finer than the values reported for the equiatomic HEAs. According to the analysis of the HEA powder particles' deformation behavior, the system operated in a ductile-brittle mode. The thermal behavior of prepared alloy, characterized by differential thermal analysis, was similar from that of equiatomic NiCoCuFeMn alloy. Similar to the equiatomic NiCoCuFeMn, the sluggish diffusion effect was not true for the Ni25Co20Cu10Fe25Mn20 HEA. Studying the magnetic behavior of Ni25Co20Cu10Fe25Mn20 HEA, using vibrating sample magnetometry, confirmed a soft magnetic behavior for this material like an equiatomic alloy.

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The data underlying this article will be shared on reasonable request to the corresponding author.

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  1. Department of New Science and Technology, Nanomaterials Group, Semnan University, Semnan, 35131-19111, Iran

    Samaneh Mamnooni & Ehsan Borhani

  2. Department of Mechanical Engineering, Faculty of Engineering, University of Kyrenia, Kyrenia, Mersin 10, Turkey

    Mehdi Shahedi Asl

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All authors contributed to the study conception and design. Material preparation, data collection and analysis were performed by Samaneh Mamnooni. The first draft of the manuscript was written by Samaneh Mamnooni. Ehsan Borhani and Mehdi Shahedi Asl commented on previous versions of the manuscript. All authors read and approved the final manuscript.

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Mamnooni, S., Borhani, E. & Shahedi Asl, M. Nanocrystalline Ni25Co20Cu10Fe25Mn20 High-Entropy Alloys Prepared by Mechanical Alloying. JOM (2024). https://doi.org/10.1007/s11837-024-06474-w

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