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A rapid voltammetric strategy for determination of ferulic acid using electrochemical nanostructure tool in food samples

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Abstract

In this project, we performed an electrochemical investigation using a reduced graphene (rG) decorated CdO nanocomposite/1-methyl-3-octylimidazolium tetrafluoroborate ionic liquid (MOITF) carbon paste electrode (rG-CdO/MOITF/CPE) for determination of ferulic acid in food samples. In preparation of rG-CdO/MOITF/CPE, 6% w/w rG-CdO nanocomposite and 20% v/v room temperature ionic liquid were used to modify the bare CPE. SEM (Scanning Electron Microscopy) and XRD (X-Ray Diffraction) methods were applied to characterize the structure of the synthesized rG-CdO nanocomposite. At all the stages of this research, phosphate buffer solution (PBS) with the pH of 5.0, as an optimized pH condition, was used. The electron transfer coefficient (α) was obtained ⁓0.68 by recorded data from cyclic voltammogram of rG-CdO/MOITF/CPE in the presence of ferulic acid. In addition, using the chronoamperometric technique, the diffusion coefficient (D) of ferulic acid at rG-CdO/MOITF/CPE was calculated 5.4 × 10−5 cm2/s. Using the square wave voltammetry method, the linear dynamic range (LDR) was calculated to be from 0.02 to 400 μM, and the limitation of detection (LOD) was obtained as 8.0 nM. Eventually, the rG-CdO/MOITF/CPE was utilized to determine the amount of ferulic acid in food samples, and statistical calculations confirmed the sensitivity, selectivity, and precision of rG-CdO/MOITF/CPE, which is an electroanalytical tool.

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  1. Department of Food Science and Technology, Ayatollah Amoli Branch, Islamic Azad University, Amol, Iran

    Peyman Ebrahimi, Seyed-Ahmad Shahidi & Majedeh Bijad

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  1. Peyman Ebrahimi
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  2. Seyed-Ahmad Shahidi
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  3. Majedeh Bijad
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Correspondence to Seyed-Ahmad Shahidi.

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Ebrahimi, P., Shahidi, SA. & Bijad, M. A rapid voltammetric strategy for determination of ferulic acid using electrochemical nanostructure tool in food samples. Food Measure 14, 3389–3396 (2020). https://doi.org/10.1007/s11694-020-00585-z

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