Abstract
Microstructural characteristics and tensile behavior of a novel hot-rolled medium-Mn steel, 0.25C-8.5Mn-0.5Si-2.5Al (wt.%), under different intercritical annealing temperatures (TIA) were evaluated. The results show that an ultrafine duplex lamellar microstructure with a maximum volume fraction of retained austenite (RA) of 65 vol.% was obtained at TIA of 750 °C. It was found that both the stability of the RA and its stability range play critical role in controlling the sustainable TRIP effect. The product of ultimate tensile strength and total elongation as high as ~ 66 GPa% was obtained at TIA of 725 °C, which is much higher than those of previously investigated medium-Mn steels with similar Mn contents, indicating a great potential for the tested steel. The analysis of the fracture surface revealed that the steel exhibited a kind of micro-delamination fracture, which was found to be primarily nucleated at the interfaces of the transformation-induced martensite and ferrite, and the micro-delamination fracture became more significant with increasing TIA.
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References
M. Takahashi, Sheet Steel Technology for the Last 100 Years: Progress in Sheet Steels in Hand with the Automobile Industry, ISIJ Int., 2015, 55, p 79–88
D.W. Suh and S.J. Kim, Medium Mn Transformation-Induced Plasticity Steels: Recent Progress and Challenges, Scr. Mater., 2017, 126, p 63–67
Y.K. Lee and J. Han, Current Opinion in Medium Manganese Steel, Mater. Sci. Technol., 2015, 31, p 843–856
H. Dong, W.Q. Cao, J. Shi, C.Y. Wang, M.Q. Wang, and Y.Q. Weng, Microstructure and Performance Control Technology of the 3rd Generation Auto Sheet Steels, Iron Steel, 2011, 46(6), p 1–11
E. De Moor, P.J. Gibbs, J.G. Speer, D.K. Matlock, and J. Schroth, Strategies for Third-Generation Advanced High-Strength Steel Development, Iron Steel Technol., 2010, 7, p 133–144
C.W. Shao, W.J. Hui, Y.J. Zhang, X.L. Zhao, and Y.Q. Weng, Microstructure and Mechanical Properties of Hot-Rolled Medium-Mn Steel Containing 3% Aluminum, Mater. Sci. Eng., A, 2017, 682, p 45–53
S.J. Lee, S.M. Shin, M.Y. Kwon, K.Y. Lee, and B.C. De Cooman, Tensile Properties of Medium Mn Steel with a Bimodal UFG α + γ and Coarse δ-Ferrite Microstructure, Metall. Mater. Trans. A, 2017, 48, p 1678–1700
Z.C. Li, H. Ding, R.D.K. Misra, Z.H. Cai, and H.X. Li, Microstructural Evolution and Deformation Behavior in the Fe-(6,8.5)Mn-3Al-0.2C TRIP Steels, Mater. Sci. Eng., A, 2016, 672, p 161–169
Z.H. Cai, H. Ding, H. Kamoutsi, G.N. Haidemenopoulos, and R.D.K. Misra, Interplay Between Deformation Behavior and Mechanical Properties of Intercritically Annealed and Tempered Medium-Manganese Transformation-Induced Plasticity Steel, Mater. Sci. Eng., A, 2016, 654, p 359–367
J. Han, S.J. Lee, J.G. Jung, and Y.K. Lee, The Effects of the Initial Martensite Microstructure on the Microstructure and Tensile Properties of Intercritically Annealed Fe-9Mn-0.05C Steel, Acta Mater., 2014, 78, p 369–377
P.J. Gibbs, E. De Moor, M.J. Merwin, B. Clausen, J.G. Speer, and D.K. Matlock, Austenite Stability Effects on Tensile Behavior of Manganese-Enriched-Austenite Transformation-Induced Plasticity Steel, Metall. Mater. Trans. A, 2011, 42, p 3691–3702
C. Wang, J. Shi, C.Y. Wang, W.J. Hui, M.Q. Wang, H. Dong, and W.Q. Cao, Development of Ultrafine Lamellar Ferrite and Austenite Duplex Structure in 0.2C5Mn Steel During ART-Annealing, ISIJ Int., 2011, 51, p 651–656
B. Hu, H.W. Luo, F. Yang, and H. Dong, Recent Progress in Medium-Mn Steels Made with New Designing Strategies, a Review, J. Mater. Sci. Technol., 2017, 33, p 1457–1464
M.H. Cai, H.S. Huang, J.H. Su, H. Ding, and P.D. Hodgson, Enhanced Tensile Properties of a Reversion Annealed 6.5Mn-TRIP Alloy via Tailoring Initial Microstructure and Cold Rolling Reduction, J. Mater. Sci. Technol., 2018, 34(8), p 1428–1435
Z.H. Cai, H. Ding, Z.Y. Ying, and R.D.K. Misra, Microstructural Evolution and Deformation Behavior of a Hot-Rolled and Heat-Treated Fe-8Mn-4Al-0.2C Steel, J. Mater. Eng. Perform., 2014, 23, p 1131–1137
S.J. Lee, S.W. Lee, and B.C. De Cooman, Mn Partitioning During the Intercritical Annealing of Ultrafine-Grained 6% Mn Transformation-Induced Plasticity Steel, Scr. Mater., 2011, 64, p 649–652
X.N. Luo, X.Y. Zhong, H.W. Luo, H.H. Zhou, C.Y. Wang, and J. Shi, Mn Diffusion at Early Stage of Intercritical Annealing of 5Mn Steel, J. Iron Steel Res. Inter., 2015, 22, p 1015–1019
R.L. Miller, Ultrafine-Grained Microstructures and Mechanical Properties of Alloy Steels, Metall. Trans. A, 1972, 3, p 905–912
M.J. Merwin, Low-Carbon Manganese TRIP Steels, Mater. Sci. Forum, 2007, 539–543, p 4327–4332
B. Hu and H.W. Luo, A Strong and Ductile 7Mn Steel Manufactured by Warm Rolling and Exhibiting Both Transformation and Twinning Induced Plasticity, J. Alloy. Compd., 2017, 725, p 684–693
D.W. Suh, S.J. Park, T.H. Lee, C.S. Oh, and S.J. Kim, Influence of Al on the Microstructural Evolution and Mechanical Behavior of Low-Carbon, Manganese Transformation-Induced-Plasticity Steel, Metall. Mater. Trans. A, 2010, 41, p 397–408
Z.H. Cai, H. Ding, R.D.K. Misra, and Z.Y. Ying, Austenite Stability and Deformation Behavior in a Cold-Rolled Transformation-Induced Plasticity Steel with Medium Manganese Content, Acta Mater., 2015, 84, p 229–236
I. Gutierrez-Urrutia and D. Raabe, Influence of Al Content and Precipitation State on the Mechanical Behavior of Austenitic High-Mn Low-Density Steels, Scr. Mater., 2013, 68, p 343–347
E. Girault, A. Mertens, P. Jacques, Y. Houbaert, B. Verlinden, and J.V. Humbeeck, Comparison of the Effects of Silicon and Aluminium on the Tensile Behaviour of Multiphase TRIP-Assisted Steels, Scr. Mater., 2001, 44, p 885–892
N.H. van Dijk, A.M. Butt, L. Zhao, J. Sietsma, S.E. Offerman, J.P. Wright, and S. van der Zwaag, Thermal Stability of Retained Austenite in TRIP Steels Studied by Synchrotron X-Ray Diffraction During Cooling, Acta Mater., 2005, 53, p 5439–5447
D.Y. Lee, J.K. Kim, S.W. Lee, K.Y. Lee, and B.C. De Cooman, Microstructures and Mechanical Properties of Ti and Mo Micro-alloyed Medium Mn Steel, Mater. Sci. Eng., A, 2017, 706, p 1–14
D.W. Suh, J.H. Ryu, M.S. Joo, H.S. Yang, K. Lee, and H.K.D.H. Bhadeshia, Medium-Alloy Manganese-Rich Transformation-Induced Plasticity Steels, Metall. Mater. Trans. A, 2013, 44A, p 286–293
S.W. Lee and B.C. De Cooman, Tensile Behavior of Intercritically Annealed Ultra-Fine Grained 8% Mn Multi-phase Steel, Steel Res. Int., 2015, 86, p 1170–1178
S.J. Park, B. Hwang, K.H. Lee, T.H. Lee, D.W. Suh, and H.N. Han, Microstructure and Tensile Behavior of Duplex Low-Density Steel Containing 5 Mass% Aluminum, Scr. Mater., 2013, 68, p 365–369
Z.C. Li, R.D.K. Misra, Z.H. Cai, H.X. Li, and H. Ding, Mechanical Properties and Deformation Behavior in Hot-Rolled 0.2C-1.5/3Al-8.5Mn-Fe TRIP Steel: The Discontinuous TRIP Effect, Mater. Sci. Eng., A, 2016, 673, p 63–72
D. Embury and O. Bouaziz, Steel-Based Composites: Driving Forces and Classification, Annu. Rev. Mater. Res., 2010, 40, p 213–241
W.J. Hui, C.W. Shao, Y.J. Zhang, X.L. Zhao, and Y.Q. Weng, Microstructure and Mechanical Properties of Medium Mn Steel Containing 3%Al Processes by Warm Rolling, Mater. Sci. Eng., A, 2017, 707, p 501–510
H.K. Choi, S.J. Lee, J.W. Lee, F. Barlat, and B.C. De Cooman, Characterization of Fracture in Medium Mn Steel, Mater. Sci. Eng., A, 2017, 687, p 200–210
M.Y. Seok, I.C. Choi, J. Moon, S. Kim, U. Ramamurty, and J.I. Jang, Estimation of the Hall-Petch Strengthening Coefficient of Steels Through Nanoindentation, Scr. Mater., 2014, 87, p 49–52
R. Zhang, W.Q. Cao, Z.J. Peng, J. Shi, H. Dong, and C.X. Huang, Intercritical Rolling Induced Ultrafine Microstructure and Excellent Mechanical Properties of the Medium-Mn Steel, Mater. Sci. Eng., A, 2013, 583, p 84–88
H.F. Xu, J. Zhao, W.Q. Cao, J. Shi, C.Y. Wang, C. Wang, J. Li, and H. Dong, Heat Treatment Effects on the Microstructure and Mechanical Properties of a Medium Manganese Steel (0.2C-5Mn), Mater. Sci. Eng., A, 2012, 532, p 435–442
J. Chiang, B. Lawrence, J.D. Boyd, and A.K. Pilkey, Effect of Microstructure on Retained Austenite Stability and Work Hardening of TRIP Steels, Mater. Sci. Eng., A, 2011, 528, p 4516–4521
J. Shi, X.J. Sun, W.Q. Wang, W.J. Hui, H. Dong, and W.Q. Cao, Enhanced Work-Hardening Behavior and Mechanical Properties in Ultrafine-Grained Steels with Large-Fractioned Metastable Austenite, Scr. Mater., 2010, 63, p 815–818
Y.H. Nie, Y. Kimura, T. Inoue, F.X. Yin, E. Akiyama, and K. Tsuzaki, Hydrogen embrittlement of a 1500-MPa tensile strength level steel with an ultrafine elongated grain structure, Metall. Mater. Trans. A, 2012, 43, p 1670–1687
J.J. Sun, T. Jiang, Y. Sun, Y.J. Wang, and Y.N. Liu, A Lamellar Structured Ultrafine Grain Ferrite-Martensite Dual Phase Steel and its Resistance to Hydrogen Embrittlement, J. Alloy. Compd., 2017, 698, p 390–399
Y.J. Zhang, W.J. Hui, J.J. Wang, M. Lei, and X.L. Zhao, Enhancing the Resistance to Hydrogen Embrittlement of Al-Containing Medium-Mn Steel Through Heavy Warm Rolling, Scr. Mater., 2019, 165, p 15–19
Q. Tonizzo, A.F. Gourgues-Lorenzon, M. Mazière, and A. Perlade, Microstructure, Plastic Flow and Fracture Behavior of Ferrite-Austenite Duplex Low Density Medium Mn Steel, Mater. Sci. Eng., A, 2017, 706, p 217–236
G. Avramovic-Cingara, C. Saleh, M.K. Jain, and D.S. Wilkinson, Void Nucleation and Growth in Dual-Phase Steel 600 During Uniaxial Tensile Testing, Metall. Mater. Trans. A, 2009, 40, p 3117–3127
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This work was supported by the Fundamental Research Funds for the Central Universities (No. 2017RC024).
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Zhang, Y., Wang, J., Xie, Z. et al. Microstructural Characteristics and Tensile Behavior of a Hot-Rolled Medium-Mn Steel (0.25C-8.5Mn-0.5Si-2.5Al) Processed by Intercritical Annealing Treatment. J. of Materi Eng and Perform 29, 2623–2634 (2020). https://doi.org/10.1007/s11665-020-04755-4
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DOI: https://doi.org/10.1007/s11665-020-04755-4