Abstract
Background
High pressure die casting (HPDC) Mg alloy has a hetero-structure in which the microstructures gradually coarsen from the casting surface to the interior, leading to the different elastic–plastic (E-P) transitional behaviors among the layers.
Objective
In this paper, we quantitively determined the diverse E-P transitions among the HPDC layers and related them to the microstructural evolution.
Methods
To investigate independently the E-P transitional behavior of the layer, the surface, middle, and central layers were deliberately sliced in sequence from the casting surface to the interior of the HPDC Mg-4Al-5.7RE (in wt.%) component. The onset and the end of E-P transition in each layer were quantitively determined by cyclic tensile test and Kocks-Mecking analysis, respectively.
Results
It was found that the plastic deformation for all layers occurred in the first unloading loop near zero strain, indicating the start of the E-P transition. With increasing strain, the E-P transition ended first in the middle layer at 0.0081 strain due to the lowest fraction of the second phases and ended last at the small-grained surface layer at 0.0090 strain. Excluding the twinning-dependent anelastic strain, the E-P transitions ended in advance at the strains of 0.0059 and 0.0062 in the middle and surface layer, respectively.
Conclusions
A combination of cyclic tensile test and Kocks-Mecking analysis provided a method to quantitively determine the diverse E-P transitions among the HPDC layers resulted from the hetero-structure regarding grains, the second phases, and twins.
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Notes
Although the Bauschinger effect does contribute to the anelasticity of the whole casting sample during deformation, the reversible twinning is still the major cause of anelasticity.
References
Luo AA (2013) Magnesium casting technology for structural applications. J Magnesium Alloys 1:2–22
B.L. Mordike, T. Ebert (2001) Magnesium: Properties - applications - potential. Mater. Sci. Eng., A 302:37–45.
Ang HQ, Abbott TB, Zhu S, Gu C, Easton MA (2016) Proof stress measurement of die-cast magnesium alloys. Materials Design 112:402–409
Agnew SR, Tomé CN, Brown DW, Holden TM, Vogel SC (2003) Study of slip mechanisms in a magnesium alloy by neutron diffraction and modeling. Scr Mater 48:1003–1008
Wang H, Wu PD, Wang J (2013) Modeling inelastic behavior of magnesium alloys during cyclic loading-unloading. Int J Plasticity 47:49–64
Ang HQ, Abbott TB, Zhu S, Easton MA (2019) An Analysis of the Tensile Deformation Behavior of Commercial Die-Cast Magnesium-Aluminum-Based Alloys. Metall Mater Trans A 50:3827–3841
H.Q. Ang, T.B. Abbott, S. Zhu, M.A. Easton (2017) Anelasticity of die-cast magnesium-aluminium based alloys under different strain rates. Mater. Sci. Eng., A 707:101–109.
K.V. Yang, C.H. Cáceres, A.V. Nagasekhar, M.A. Easton (2012) The skin effect and the yielding behavior of cold chamber high pressure die cast Mg-Al alloys. Mater. Sci. Eng., A 542:49–55.
K.V. Yang, C.H. Cáceres, M.A. Easton (2013) A microplasticity-based definition of the skin in HPDC Mg-Al alloys. Mater. Sci. Eng., A 580:355–361.
Zhang B (2016) Numerical Analysis of Skin Effect on Microplastic Flow of HPDC Mg Alloys. Adv Eng Mater 18:1273–1279
Ji S, Yang H, Cui X, Fan Z (2017) Macro-heterogeneities in microstructures, concentrations, defects and tensile properties of die cast Al-Mg-Si alloys. Mater Sci Tech-Lond 33:2223–2233
K.V. Yang, M.A. Easton, C.H. Cáceres (2013) The development of the skin in HPDC Mg-Al alloys. Mater. Sci. Eng., A 580:191–195.
Wei J, Wang Q, Yin D, Zhang L, Zhou H, Ye B, Jiang H, Ding W (2020) Extra Strain Hardening in High Pressure Die Casting Mg-Al-RE Alloy. Metall Mater Trans A 51:1487–1492
Dai J, Easton M, Zhu S, Wu G, Ding W (2012) Grain refinement of Mg-10Gd alloy by Al additions. J Mater Res 27:2790–2797
G.E. Mann, T. Sumitomo, C.H. Cáceres, J.R. Griffiths (2007) Reversible plastic strain during cyclic loading-unloading of Mg and Mg-Zn alloys. Mater. Sci. Eng., A 456:138–146.
Zhang L, Wang Q, Liao W, Guo W, Ye B, Li W, Jiang H, Ding W (2017) Effects of cyclic extrusion and compression on the microstructure and mechanical properties of AZ91D magnesium composites reinforced by SiC nanoparticles. Mater Charact 126:17–27
Cáceres CH, Sumitomo T, Veidt M (2003) Pseudoelastic behaviour of cast magnesium AZ91 alloy under cyclic loading–unloading. Acta Mater 51:6211–6218
Sumitomo T, Cáceres CH, Veidt M (2002) The elastic modulus of cast Mg-Al-Zn alloys. J Light Met 2:49–56
Meyers MA, Chawla KK (2008) Mechanical Behavior of Materials. Cambridge University Press
Cáceres CH, Lukáč P (2008) Strain hardening behaviour and the Taylor factor of pure magnesium. Philos Mag 88:977–989
Kocks UF, Mecking H (2003) Physics and phenomenology of strain hardening: the FCC case. Prog Mater Sci 48:171–273
Cáceres CH, Lukáč P, Blake A (2008) Strain hardening due to 10 12 twinning in pure magnesium. Philos Mag 88:991–1003
C.H. Cáceres, A.H. Blake (2007) On the strain hardening behaviour of magnesium at room temperature. Mater. Sci. Eng., A 462:193–196.
Mathaudhu SN, Sillekens WH, Neelameggham NR, Hort N (2012) Magnesium Technology 2012. John Wiley & Sons
Agnew SR, Tomé CN, Brown DW, Holden TM, Vogel SC (2003) Study of slip mechanisms in a magnesium alloy by neutron diffraction and modeling. Scr. Mater. 48:1003–1008
Hutchinson WB, Barnett MR (2010) Effective values of critical resolved shear stress for slip in polycrystalline magnesium and other hcp metals. Scr Mater 63:737–740
M.F. Savage, J. Tatalovich, M. Zupan, K.J. Hemker, M.J. Mills (2001) Deformation mechanisms and microtensile behavior of single colony Ti–6242Si. Mater. Sci. Eng., A 319–321:398–403.
Gong J, Wilkinson AJ (2011) A microcantilever investigation of size effect, solid-solution strengthening and second-phase strengthening for <a> prism slip in alpha-Ti. Acta Mater 59:5970–5981
Wu X, Yang M, Yuan F, Wu G, Wei Y, Huang X, Zhu Y (2015) Heterogeneous lamella structure unites ultrafine-grain strength with coarse-grain ductility. Proc Natl Acad Sci 112:14501–14505
Wu X, Zhu Y (2017) Heterogeneous materials: a new class of materials with unprecedented mechanical properties. Mater Res Lett 5:527–532
Zhu Y, Wu X (2019) Perspective on hetero-deformation induced (HDI) hardening and back stress. Mater Res Lett 7:393–398
Gharghouri MA, Weatherly GC, Embury JD, Root J (1999) Study of the mechanical properties of Mg-7.7 at.% Al by in-situ neutron diffraction. Philos Mag A 79:1671–1695
V.S. Tong, E. Wielewski, B. Britton (2018) Characterisation of slip and twinning in high rate deformed zirconium with electron backscatter diffraction. arXiv preprint https://arxiv.org/abs/1803.00236
D. Nagarajan, X. Ren, C.H. Cáceres (2017) Anelastic behavior of Mg-Al and Mg-Zn solid solutions. Mater. Sci. Eng., A 696:387–392.
Muránsky O, Barnett MR, Carr DG, Vogel SC, Oliver EC (2010) Investigation of deformation twinning in a fine-grained and coarse-grained ZM20 Mg alloy: Combined in situ neutron diffraction and acoustic emission. Acta Mater 58:1503–1517
Partridge PG (1967) The crystallography and deformation modes of hexagonal close-packed metals. Metallurgical Reviews 12:169–194
Acknowledgments
This work was supported by the National Key Research and Development Program of China (Grant No. 2016YFB0301001) and the National Natural Science Foundation of China (NSFC, Grant Nos. U1902220 and 51674166).
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Wei, J., Wang, Q.D., Ebrahimi, M. et al. Experimental Study on the Elastic–plastic Transitions of the Hetero-structured High Pressure Die Casting Mg–Al-RE Alloy. Exp Mech 61, 1143–1152 (2021). https://doi.org/10.1007/s11340-021-00724-7
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DOI: https://doi.org/10.1007/s11340-021-00724-7