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Facile synthesis of mesoporous carbons with tailored porosity by a fast polymerization

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Abstract

Mesoporous carbons (MCs) with controllable pore structure and pore size have been prepared by direct carbonization of composites of reverse compolymer-phloroglucinol/formaldehyde. The microstructure of the MCs was analyzed by small-angle X-ray scattering, nitrogen adsorption isotherms and transmission electron microscope. The results showed the pore size of the obtained MCs can be easily tuned from 6.4 to 11.4 nm. Furthermore, the inkbottle-like or cylindrical pore structure of MCs can be obtained by simply adjusting the ratios of formaldehyde and phloroglucinol.

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Acknowledgements

The research was supported by the financial support of the Shanxi Province Foundation for Youths (2015021072), the Program for the Innovative Talents of Taiyuan Institute of Technology (TITXD201403), Special Youth Science and Technology Innovation (QKCZ201635), National Training Programs of Innovation and Entrepreneurship for Undergraduates (201614101004). Greatly thanks Fund of Testing from Institute of High Energy and Physics for SAXS measurements assistance.

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Authors and Affiliations

  1. Department of Materials Enginnering, Taiyuan Institute of Technology, Taiyuan, 030008, Shanxi, China

    Huidi Yang, Peng Li, Xiaoxiao Ma & Lidong Zhao

  2. Materials Science and Engineering School, North University of China, Taiyuan, 030051, China

    Xiaoxiao Ma

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  1. Huidi Yang
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  2. Peng Li
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  3. Xiaoxiao Ma
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  4. Lidong Zhao
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Correspondence to Peng Li.

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Yang, H., Li, P., Ma, X. et al. Facile synthesis of mesoporous carbons with tailored porosity by a fast polymerization. J Porous Mater 26, 561–565 (2019). https://doi.org/10.1007/s10934-018-0652-x

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  • DOI: https://doi.org/10.1007/s10934-018-0652-x

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