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Dynamic Light Scattering and Image Analysis of FePt Based Nanoparticles from Size-Selective Precipitation

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Abstract

Nanoseparation was performed on iron-platinum based nanoparticles from the reaction between iron(III) tris(2,2,6,6-tetramethyl-3,5-heptanedionate) and platinum(II) acetylacetonate. Dynamic Light Scattering (DLS) provided a rapid and effective technique to monitor the classification of these polydisperse nanoparticles. After the size-selective precipitation, the nanoparticles were separated into 2 groups with different hydrodynamic diameters. In additions, the storage time and additional surfactants also increased the size distribution of nanoparticles. After the repeated size-selective precipitation, the hydrodynamic diameter was reduced to 7.8 nm and the particle diameter of 3.4 nm was averaged from Transmission Electron Microscopy (TEM). Furthermore, the TEM image processing was used to demonstrate the correlation between the size distribution of nanoparticles from the repeated size-selective precipitation and their self-assembly on liquid as well as solid substrates.

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Acknowledgments

This work is funded by the Thailand Excellent Center in Physics under Grant Number ThEP-60-PIP-WU3. This research was partially supported by the New Strategic Research (P2P) project, Walailak University, Thailand. The authors would like to thank P. Harding of Walailak University for her suggestions. The technical assistance in TEM imaging by P. Pinsrithong of Scientific Equipment Center, Prince of Songkla University, is acknowledged.

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Authors and Affiliations

  1. Division of Physics, School of Science, Walailak University, Nakhon Si Thammarat, 80160, Thailand

    Pharunee Sarmphim, Kasidapa Polprasarn & Chitnarong Sirisathitkul

  2. School of Informatics, Walailak University, Nakhon Si Thammarat, 80160, Thailand

    Yaowarat Sirisathitkul

  3. Functional Materials and Nanotechnology Center of Excellence, Walailak University, Nakhon Si Thammarat, 80160, Thailand

    Chitnarong Sirisathitkul

  4. Thailand Center of Excellence in Physics, Commission on Higher Education, Bangkok, 10400, Thailand

    Chitnarong Sirisathitkul

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  1. Pharunee Sarmphim
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  2. Yaowarat Sirisathitkul
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Correspondence to Yaowarat Sirisathitkul.

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Sarmphim, P., Sirisathitkul, Y., Polprasarn, K. et al. Dynamic Light Scattering and Image Analysis of FePt Based Nanoparticles from Size-Selective Precipitation. J Clust Sci 31, 421–428 (2020). https://doi.org/10.1007/s10876-019-01655-z

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  • DOI: https://doi.org/10.1007/s10876-019-01655-z

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