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Mossbauer spectroscopy study of Fe@ZrO2 nanocomposites formation by MA SHS technology

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Abstract

Particles with core-in-shell structure Fe@ZrO2 were synthesized by step-by-step technology including formation of mechanically pre-activated (MA) precursors with Fe/Zr and Fe2O3/[Fe/Zr] composite structures formation following by Self-Propagated High temperature synthesis (SHS). Mossbauer spectroscopy, Transmission and Scanning electron Microscopy have been performed to study the peculiarities of local structure and its evolution through the sequential synthesis steps via various milling periods and reagent compositions. The exact conditions for iron core in oxide shell Fe@ZrO2 structure formation with promising functionality has been established.

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Acknowledgements

This work was supported by the Siberian Branch of the Russian Academy of Sciences, the National Academy of Science of Belarus and Moscow University Program of Development.

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Authors and Affiliations

  1. Department of Physics, Moscow M.V. Lomonosov State University, Moscow, Russia

    Tatiana Kiseleva & Alla Novakova

  2. Institute of Powder Metallurgy NAS, Minsk, Belarus

    Alexey Letsko & Tatiana Talako

  3. United Institute of Mechanical Engineering, Minsk, Belarus

    Svetlana Kovaleva

  4. Institute of Solid State Chemistry and Mechanochemistry RAS, Novosibirsk, Russia

    Tatiana Grigoreva & Nikolay Lyakhov

Authors
  1. Tatiana Kiseleva
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  2. Alexey Letsko
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  3. Tatiana Talako
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  4. Svetlana Kovaleva
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  5. Tatiana Grigoreva
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  6. Alla Novakova
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  7. Nikolay Lyakhov
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Corresponding author

Correspondence to Tatiana Kiseleva.

Additional information

This article is part of the Topical Collection on Proceedings of the International Conference on the Applications of the Mössbauer Effect (ICAME 2017), Saint-Petersburg, Russia, 3–8 September 2017

Edited by Valentin Semenov

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Kiseleva, T., Letsko, A., Talako, T. et al. Mossbauer spectroscopy study of Fe@ZrO2 nanocomposites formation by MA SHS technology. Hyperfine Interact 239, 14 (2018). https://doi.org/10.1007/s10751-018-1490-6

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