Skip to main content
Log in

Investigations on the structure and properties of palm leaf sheath fiber

  • Original Paper
  • Published:
Cellulose Aims and scope Submit manuscript

Abstract

As a natural cellulosic fiber, palm leaf sheath fiber (palm fiber) is widely-distributed and abundant cellulose and engineering fiber resource. To obtain essential information about palm fiber, its morphology, composition, chemical and crystal structure, tensile characteristic and adsorption property were investigated. Test results of palm fiber were compared with those of other natural cellulosic fibers. Palm fiber presents aligned Si-dots on the surface and abundant fiber cells with spiral vessel tissues at the cross section. The chemical composition reveals that palm fiber contains abundant lignin but smaller amount of cellulose (the content of 28.16 %). In addition, investigation illustrates that cellulose in palm fiber is Iβ-dominant type, which is also confirmed by FTIR analysis. X-ray diffraction study shows that the crystallinity (30.52 %), crystallinity index (36.5 %) and crystal size (2.5 nm) are all apparently lower than those of ramie, flax and bamboo fibers. Given the low crystallinity and cellulose content of palm fiber, its tensile strength and Young’s modulus are also lower than those of other fibers. Moreover, palm fiber exhibits excellent breaking elongation, high moisture regain, distinct yield characteristic, and variability in strength. The modified Weibull model was used to study the tensile behavior of palm fiber. This model accurately predicted fiber strength. The absorption volume in isotherm of carbonized palm fiber increases with rising pressure, thus indicating good porous structure of the fiber.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Fig. 1
Fig. 2
Fig. 3
Fig. 4
Fig. 5
Fig. 6
Fig. 7
Fig. 8
Fig. 9
Fig. 10
Fig. 11

Similar content being viewed by others

References

  • Andersons J, Poriķe E, Spārniņš E (2011) Modeling strength scatter of elementary flax fibers: the effect of mechanical damage and geometrical characteristics. Compos A 42:543–549

    Article  Google Scholar 

  • Avelar FF, Bianchi ML (2010) The use of piassava fibers (Attalea funifera) in the preparation of activated carbon. Bioresour Technol 101:4639–4645

    Article  CAS  Google Scholar 

  • Baley C (2002) Analysis of the flax fibers tensile behaviour and analysis of the tensile stiffness increase. Compos A 33:939–948

    Article  Google Scholar 

  • Belaadi A, Bezazi A, Bourchak M (2013) Tensile static and fatigue behaviour of sisal fibres. Mater Des 46:76–83

    Article  Google Scholar 

  • Cantero G, Arbelaiz A, Mondragon I (2003) Effects of fiber treatment on wettability and mechanical behaviour of flax/polypropylene composites. Compos Sci Technol 63:1247–1254

    Article  CAS  Google Scholar 

  • Catauro M, Bollino F, Papale F, Gallicchio M, Pacifico S (2015) Influence of the polymer amount on bioactivity and biocompatibility of SiO2/PEG hybrid materials synthesized by sol-gel technique. Mater Sci Eng C 48:548–555

    Article  CAS  Google Scholar 

  • Charlet K, Eve S, Jernot JP (2009) Tensile deformation of a flax fiber. Proced Eng 1:233–236

    Article  Google Scholar 

  • Chawla N, Kerr M, Chawla KK (2005) Monotonic and cyclic fatigue behavior of high performance ceramic fibers. J Am Ceram Soc 88:101–108

    Article  CAS  Google Scholar 

  • Cheng L, Zhang TH, Guo M (2014) Structural characteristics and properties of windmill palm leaf sheath fiber. Wood Fiber Sci 46:270–279

    CAS  Google Scholar 

  • Christina PJ, Rudall PJ, Gregory M (2004) Systematics and biology of silica bodies in monocotyledons. Bot Rev 69:377–440

    Google Scholar 

  • Cordeiro N, Gouveia C, Moraes AGO (2011) Natural fibers characterization by inverse gas chromatography. Carbohydr Polym 84:110–117

    Article  CAS  Google Scholar 

  • d’Almeida JRM, Aquino RCMP, Monteiro SN (2006) Tensile mechanical properties morphological aspects and chemical characterization of piassava (Attalea funifera) fibers. Compos A 37:1473–1479

    Article  Google Scholar 

  • Dai Z (2008) The design of a new kind of fiber mattress based on composites and its mechanics analysis. Sci Technol Innov Her 12:150–151

    Google Scholar 

  • Devshony S, Eteshola E, Shani A (1992) Characteristics and some potential applications of date palm seeds and seed oil. JAOCS 69:595–597

    CAS  Google Scholar 

  • Focher B, Palma MT, Canetti M, Torri G, Cosentino C (2001) Structural differences between non-wood plant celluloses: evidence from solid state NMR, vibrational spectroscopy and X-ray diffractometry. Ind Crops Prod 13:193–208

    Article  CAS  Google Scholar 

  • French AD (2014) Idealized powder diffraction patterns for cellulose polymorphs. Cellulose 21:885–896

    Article  CAS  Google Scholar 

  • Ganner T, Aschl T, Eibinger M (2014) Tunable mixed amorphous-crystalline cellulose substrates (MACS) for dynamic degradation studies by atomic force microscopy in liquid environments. Cellulose 21:3927–3939

    Article  CAS  Google Scholar 

  • Greenberg AR, Mehlign A, Lee M (1989) Tensile behaviour of grass. J Mater Sci 24:2549–2554

    Article  Google Scholar 

  • Guo M, Zhang TH, Chen BW (2014) Tensile strength analysis of palm fiber leaf sheath fiber with Weibll distribution. Compos A 62:45–51

    Article  CAS  Google Scholar 

  • He JX, Tang YY, Wang SY (2007) Differences in morphological characteristics of bamboo fibers and other natural cellulose fibers: studies on X-ray diffraction, solid state 13C-CP/MAS NMR, and second derivative FTIR spectroscopy data. Iran Polym J 16:807–818

    CAS  Google Scholar 

  • Jiang XM, He WP (1992) Concise identification of infrared spectroscopy. Guangxi Normal University Press, Guilin

    Google Scholar 

  • Kerr M, Chawla N, Chawla KK (2005) Cyclic fatigue of high performance fibers. JOM 2:67–70

    Article  Google Scholar 

  • Li RQ, Song JC (2005) Measuring techniques for textile materials. Donghua University Press, Shanghai

    Google Scholar 

  • Mahesh KPO, Kuo DH, Huang BR (2015) Facile synthesis of heterostructured Ag-deposited SiO2@TiO2 composite spheres with enhanced catalytic activity towards the photodegradation of AB 1 dye. J Mol Catal A Chem 396:290–296

    Article  CAS  Google Scholar 

  • Maunder M, Lyte B, Dransfield J (2001) The conservation value of botanic garden palm collections. Biol Conserv 98:259–271

    Article  Google Scholar 

  • Methacanon P, Sumransin N (2010) Properties and potential application of the selected natural fibers as limited life geotextiles. Carbohydr Polym 82:1090–1096

    Article  CAS  Google Scholar 

  • Mortazavi SM, Moghadda MK (2010) An analysis of structure and properties of a natural cellulosic fiber (Leafiran). Fibers Polym 11:877–882

    Article  CAS  Google Scholar 

  • Munawar SS, Umemura K, Kawai S (2007) Characterization of the morphological, physical, and mechanical properties of seven nonwood plant fiber bundles. J Wood Sci 53:108–113

    Article  Google Scholar 

  • O’Sullivan AC (1997) Cellulose: the structure slowly unravels. Cellulose 4:173–207

    Article  Google Scholar 

  • Oudiani AE, Chaabouni Y, Msahli S, Sakli F (2011) Crystal transition from cellulose I to cellulose II in NaOH treated Agave americana L. fibre. Carbohydr Polym 86:1221–1229

    Article  Google Scholar 

  • Qian TT, Li JH, Ma HG, Yang J (2015) The preparation of a green shape-stabilized composite phase change material of polyethylene glycol/SiO2 with enhanced thermal performance based on oil shale ash via temperature-assisted sol-gel method. Sol Energy Mater Sol Cells 132:29–39

    Article  CAS  Google Scholar 

  • Roy A, Chakraborty S, Kundu SP (2012) Improvement in mechanical properties of jute fibres through mild alkali treatment as demonstrated by utilisation of the Weibull distribution model. Bioresour Technol 107:222–228

    Article  CAS  Google Scholar 

  • Segal L, Creely L, Martin AE, Conrad CM (1959) An empirical method for estimating the degree of crystallinity of native cellulose using X-ray diffractometer. Text Res J 29:786–794

    Article  CAS  Google Scholar 

  • Silva FA, Chawla N, Toledo Filho RD (2008) Tensile behavior of high performance natural (Sisal) fibers. Compos Sci Techno 68:3438–3443

    Article  CAS  Google Scholar 

  • Silva FA, Chawla N, Filho RDT (2009) An experimental investigation of the fatigue behavior of sisal fibers. Mater Sci Eng A 516:90–95

    Article  Google Scholar 

  • Silva FA, Chawla N, Toledo Filho RD (2010) Mechanical behavior of natural sisal fibers. J Biobased Mater Bioenergy 4:106–113

    Article  CAS  Google Scholar 

  • Sing KSW, Everett DH, Haul RAW (1985) Reporting physisorption data for gas/solid systems with special reference to the determination of surface area and porosity. Pure Appl Chem 57:603–619

    Article  CAS  Google Scholar 

  • Sugiyama J, Persson J, Chanzy H (1991) Combined infrared and electron diffraction study of the polymorphism of native cellulose. Macromolecules 24:2461–2466

    Article  CAS  Google Scholar 

  • Summerscales J, Dissanayake PJ, Virk S (2010) A review of bast fibers and their composites. Part 1: fibers as reinforcements. Compos A 41:1329–1335

    Article  Google Scholar 

  • Thygesen A, Oddershede J, Lilholt H, Thomsen AB, Ståhl K (2005) On the determination of crystallinity and cellulose content in plant fibers. Cellulose 12:563–576

    Article  CAS  Google Scholar 

  • Tomczak F (2007) Studies on lignocellulosic fibers of Brazil. Part II: morphology and properties of Brazilian coconut fibers. Compos A 38:1710–1721

    Article  Google Scholar 

  • Wang YP, Wang G, Cheng HT, Tian GL, Liu Z, Xiao QF, Zhou XQ, Han XJ, Gao XS (2010) Structures of bamboo fiber for textiles. Text Res J 80:334–343

    Article  Google Scholar 

  • Xia ZP, Yu JY, Cheng LD (2009) Study on the breaking strength of jute fibers using modified Weibull distribution. Compos A 40:54–59

    Article  Google Scholar 

  • Yang KB, Peng JH (2010) Preparation of high surface area activated carbon from coconut shells using microwave heating. Bioresour Technol 101:6163–6169

    Article  CAS  Google Scholar 

  • Yu Y, Wang HK, Lu F (2014) Bamboo fibers for composite applications: a mechanical and morphological investigation. J Mater Sci 49:2559–2566

    Article  CAS  Google Scholar 

  • Zhai S (2010) Structural, chemical and physical properties of palms fiber. Dissertation, Nanjing Forestry University

  • Zhang TH, Li XL, Cheng L (2010) Properties and application status of palm fiber. Tech Text 6:35–38

    Google Scholar 

Download references

Acknowledgments

This work was supported by the Science Foundation of Southwest University (SWUB2008049), the Fundamental Research Funds for the Central Universities (XDJK2012D008, XDJK2013A021 and XDJK2015D006) and the Postgraduates Scientific Research Innovation Project in Chongqing (CYB14057).

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to Tonghua Zhang.

Additional information

Tonghua Zhang and Min Guo are the first author of this study.

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Zhang, T., Guo, M., Cheng, L. et al. Investigations on the structure and properties of palm leaf sheath fiber. Cellulose 22, 1039–1051 (2015). https://doi.org/10.1007/s10570-015-0570-x

Download citation

  • Received:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s10570-015-0570-x

Keywords

Navigation