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Electrochemical analysis of organic compounds in solid-state: applications of voltammetry of immobilized microparticles in bioanalysis and cultural heritage science

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Abstract

Most of the advances in the electrochemical study of solid materials are due to the development and application of voltammetry of immobilized microparticles in several areas besides electroanalytical. The technique has been applied in the evaluation of solid-state electrochemical behavior of compounds, qualitative and semi-quantitative determinations, monitoring of products derived from specific reactions, authentication and discrimination of several samples, and as quality control analytical tool. Recently, the studies involving solid organic compounds in different areas, such as pharmaceutical, biomedical, food, and cultural heritage sciences, have emerged and deserved special attention. In this regard, this paper aims to review the state-of-the-art of voltammetry of immobilized microparticles applied to organic compound analysis in solid-state in several research fields, highlighting some technique features and their applications for different purposes.

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Acknowledgments

We would like to thank CAB English Lessons for the English correction.

Funding

The authors acknowledge the financial support provided by the Fundação de Amparo à Pesquisa do Estado de São Paulo, FAPESP (grant nos. 2018/13496-8 and 2018/06478-3) and the Instituto Nacional de Ciência e Tecnologia em Bioanalítica, INCTBio (grant no. 2014/50867-3 - FAPESP).

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Authors and Affiliations

  1. Institute of Chemistry, State University of Campinas, Rua Josué de Castro 126 Cidade Universitária, Campinas, SP, 130810361, Brazil

    Géssica Domingos da Silveira & José Alberto Fracassi da Silva

  2. Center for Cultural Heritage Technology (CCHT), Istituto Italiano di Tecnologia (IIT), Via della Libertà 12, Marghera, 30175, Venice, Italy

    Francesca Di Turo

  3. Laboratório de Eletro-Espectro Analítica (LEEA), Escola de Química e Alimentos, Universidade Federal do Rio Grande, Av. Itália km 8, Rio Grande, RS, 96203-900, Brazil

    Daiane Dias

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  1. Géssica Domingos da Silveira
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  2. Francesca Di Turo
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  3. Daiane Dias
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  4. José Alberto Fracassi da Silva
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Correspondence to Géssica Domingos da Silveira.

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Personal dedication: The authors would like to dedicate this to Professor Fritz Scholz on the occasion of his 65th birthday.

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da Silveira, G.D., Di Turo, F., Dias, D. et al. Electrochemical analysis of organic compounds in solid-state: applications of voltammetry of immobilized microparticles in bioanalysis and cultural heritage science. J Solid State Electrochem 24, 2633–2652 (2020). https://doi.org/10.1007/s10008-020-04720-0

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