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Synthesis and characterization of optically active magnetic PAI/Fe3O4 nanocomposites

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Abstract

This work presents the preparation and characterization of hybrid organic–inorganic optically active poly(amide–imide)/nano–Fe3O4 composites with different amount of modified Fe3O4 nanoparticles as new nanocomposites by ultrasonic irradiation and characterized by Fourier transform infrared spectra, X-ray diffraction, scanning electron microscopy (SEM), thermogravimetric analysis and vibrating sample magnetometry. The surface of Fe3O4 nanoparticles was modified with 3-aminopropyltriethoxyl silane because of the homogeneous distribution of nano-Fe3O4 in polymer matrix, which the SEM results confirmed that the Fe3O4 nanoparticles were dispersed uniformly in polymer matrix. Furthermore, as compared with pure polymer, thermogravimetric analysis data indicated an improvement of thermal stability of nanocomposites.

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Acknowledgements

We wish to express our gratitude to the Yasouj University for financial assistance.

Funding

The work was supported by the Yasouj University Foundation.

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Authors and Affiliations

  1. Department of Chemistry, Yasouj University, Yasouj, 75918-74831, Islamic Republic of Iran

    Zahra Rafiee & Zahra Panji

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  1. Zahra Rafiee
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  2. Zahra Panji
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Correspondence to Zahra Rafiee.

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This is an original article and as such does not contain any studies with human participants or animals performed by any of the authors.

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Handling Editor: H. S. Sharma.

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Rafiee, Z., Panji, Z. Synthesis and characterization of optically active magnetic PAI/Fe3O4 nanocomposites. Amino Acids 50, 1007–1012 (2018). https://doi.org/10.1007/s00726-018-2577-8

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  • DOI: https://doi.org/10.1007/s00726-018-2577-8

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