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Surface and electrochemical characterization of boron-doped diamond electrodes prepared under different conditions

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Abstract

In this study, physical, chemical, and electrochemical properties of lab-made boron-doped diamond electrodes (BDDE) prepared by hot filaments chemical vapor deposition under different conditions have been investigated. The B/C ratio in the gas phase varied in the range of 0–20,000 ppm and the content of CH4 in H2 was changed in the interval of 0.5–2 %. Scanning electron microscopy and Raman spectroscopy were used for characterization of BDD films. Cyclic voltammetry and electrochemical impedance spectroscopy of the redox system [Fe(CN)6]3−/4− were used for electrochemical characterization of prepared electrodes. Finally, all BDDEs in combination with differential pulse voltammetry were tested for herbicide linuron determination under optimized experimental conditions.

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Acknowledgments

This work was supported by The Ministry of Education, Youth and Sports of the Czech Republic (project No. CZ.1.07/2.3.00/30.0021), by the University of Pardubice (project No. SGSFChT_2015006), by grant of MŠ SR VEGA (project No. 1/0785/14), and grant of SRDA (project No. APVV-0365-12).

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Authors and Affiliations

  1. Institute of Environmental and Chemical Engineering, University of Pardubice, Studentská 573, 532 10, Pardubice, Czech Republic

    Renáta Šelešovská, Michaela Štěpánková, Lenka Janíková & Kateřina Nováková

  2. J. Heyrovsky Institute of Physical Chemistry of the AS CR, v.v.i, Dolejškova 3, 182 23, Prague 8, Czech Republic

    Kateřina Nováková

  3. Faculty of Electrical Engineering and Information Technology, Institute of Electronics and Photonics, Slovak University of Technology in Bratislava, Ilkovičova 3, 812 19, Bratislava, Slovak Republic

    Marian Vojs, Marián Marton & Miroslav Behúl

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  1. Renáta Šelešovská
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  2. Michaela Štěpánková
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  3. Lenka Janíková
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  4. Kateřina Nováková
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  5. Marian Vojs
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  7. Miroslav Behúl
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Correspondence to Renáta Šelešovská.

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Šelešovská, R., Štěpánková, M., Janíková, L. et al. Surface and electrochemical characterization of boron-doped diamond electrodes prepared under different conditions. Monatsh Chem 147, 1353–1364 (2016). https://doi.org/10.1007/s00706-015-1640-3

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  • DOI: https://doi.org/10.1007/s00706-015-1640-3

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