Abstract
Due to their high thermal stability under severe working conditions and harsh environment, nickel (Ni)-based superalloys, such as Inconel 718, Inconel 738, GTD11, and René 40, are largely used in gas turbine industry. The gamma prime (γʹ) precipitates, that are coherent with the gamma (γ) matrix in these superalloys, provide excellent mechanical properties at high operating temperatures. However, after a long time of functioning, (γʹ) precipitates coarsen and lose their coherency with the matrix, which causes damages in gas turbine blades. The main purpose of this paper is to study the effect of both solid solution and aging heat treatments temperatures on the microstructural evolution in an Inconel 738 superalloy blade, which was received after few tens of thousands of service hours. The resulting microstructures were analyzed by using scanning electron microscopy and optical microscopy along with Vickers microhardness measurements. The obtained results show that the Vickers microhardness of the studied superalloy is related to size, shape, volume fraction, and distribution of the hardening phase (γʹ) [Ni3(Al, Ti)], and to its carbides as well. It was found that the microstructural stability is related to the working temperature.
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References
M. Durand-Charre, The Microstructure of Superalloys (Routledge, London, 2017)
V.M. Imayev, S.K. Mukhtarov, A.V. Logunov, A.A. Ganeev, R.V. Shakhov, L.R. Shaikhutdinova, R.M. Imayev, Effect of thermo mechanical treatment on the microstructure and mechanical properties of a nickel base superalloy heavily alloyed with substitution elements. Lett. Mater. 9(4), 465–469 (2019)
A. Hazotte, J. Lacaze, Quantitative analysis of the microstructure of single crystal nickel-based superalloys. Acta Stereol. 16, 281–286 (1997)
F. Pettinari, M. Jouiad, P. Caron, et al., Influence of the solute nature on the tensile behaviour and on the microstructure of γ-phases of nickel based superalloys. Revue de Metallurgie. Cahiers D'Informations Techniques, pp. 1038–1046 (2000)
J. Cormier, J.-Y. Guedou. Ma1-des materiaux incontournables pour les turboreacteurs aeronautiques: les superalliages base nickel (2015)
A. Ghasemi, M. Pouranvari, Thermal processing strategies enabling boride dissolution and gamma prime precipitation in dissimilar nickel-based superalloys transient liquid phase bond. Mater. Des. 182, 108008 (2019)
T.M. Pollock, S. Tin, Nickel-based superalloys for advanced turbine engines: chemistry, microstructure and properties. J. Propuls. Power. 22, 361–374 (2006)
T.M. Pollock, Alloy design for aircraft engines. Nat. Mater. 15, 809–815 (2016)
C. Kim, Creep damage characterization of Ni-based superalloy by acoustic nonlinearity. Prog. Nat. Sci. Mater. Int. 22(4), 303–310 (2012)
J.A. Villada, R.G. Bayro-Lazcano, E. Martinez-Franco, D.G. Espinosa-Arbelaez, J. Gonzalez-Hernandez, J.M. Alvarado-Orozco, Relationship between γ′ phase degradation and in-service GTD-111 first-stage blade local temperature. J. Mater. Eng. Perform. 28(4), 1950–1957 (2019)
Y.K. Kim, D. Kim, H.-K. Kim et al., An intermediate temperature creep model for Ni-based superalloys. Int. J. Plast. 79, 153–175 (2016)
D.A. Woodford, Environmental damage of a cast nickel base superalloy. Metall. Trans. A 12(2), 299–308 (1981)
J.A. Pfaendtner, C.J. McMahon Jr., Oxygen-induced intergranular cracking of a Ni-base alloy at elevated temperatures—an example of dynamic embrittlement. Acta Mater. 49(16), 3369–3377 (2001)
F. Sun, J. Tong, Q. Feng et al., Microstructural evolution and deformation features in gas turbine blades operated in-service. J. Alloys. Compd. 618, 728–733 (2015)
K.-H. Chang, Design Theory and Methods Using CAD/CAE: The Computer Aided Engineering Design Series (Academic Press, Cambridge, 2014)
H.E. Collins, R.J. Quigg, Carbide and intermetallic instability in advanced nickel-base superalloys (Relative stability of gamma prime and minor phases in five nickel base superalloys, discussing effect of time, aging temperature and stress). ASM Trans. Q. 61, 139–148 (1968)
L. Gong, B. Chen, Z. Du, M. Zhang et al., Investigation of solidification and segregation characteristics of cast Ni-base superalloy K417G. J. Mater. Sci. Technol. 34(3), 541–550 (2018)
P. Kontis, A. Kostka, D. Raabe et al., Influence of composition and precipitation evolution on damage at grain boundaries in a crept polycrystalline Ni-based superalloy. Acta Mater. 166, 158–167 (2019)
G. Bai, J. Li, R. Hu et al., Effect of thermal exposure on the stability of carbides in Ni–Cr–W based superalloy. Mater. Sci. Eng. A 528(6), 2339–2344 (2011)
Q. Wu, Microstructural evolution in advanced boiler materials for ultra-supercritical coal power plants. Thèse de doctorat, University of Cincinnati (2006)
S. Cruchley, H. Evans, M. Taylor, An overview of the oxidation of Ni-based superalloys for turbine disc applications: surface condition, applied load and mechanical performance. Mater. High Temper. 33(4–5), 465–475 (2016)
E.W. Ross, René 100: a sigma-free turbine blade alloy. JOM 19(12), 12–14 (1967)
J. Capponi, C. Chaillout, A. Hewat, P. Lejay, M. Marezio, N. Nguyen, B. Raveau, J. Soubeyroux, J. Tholence, R. Tournier, EPL (Europhys Lett) 3, 1301 (1987)
M. Revaud, Optimisation métallurgique du superalliage à base de Nickel 718Plus Ph.D. thesis Ecole Nationale Supérieure des Mines de Paris (2013)
J.R. Davis, et al. (eds.), Nickel, Cobalt, and their Alloys (ASM International, Cleveland, 2000)
E.F. Bradley, (ed.), Superalloys: a technical guide (ASM International, Materials Park, Ohio, 1988)
D.J. Tillack, ASM Handbook, vol. 4 (ASM International, Materials Park, 1993), pp. 907–912
A. James, Review of rejuvenation process for nickel base superalloys. Mater. Sci. Technol. 17(5), 481–486 (2001)
P. Wangyao, N. Chuankrerkkul, S. Polsilapa et al., Gamma prime phase stability after long-term thermal exposure in cast nickel based superalloy, IN-738. Chiang Mai J. Sci. 36(3), 312–319 (2009)
P. Wangyao, V. Krongtong, N. Panich et al., Effect of 12 heat treatment conditions after HIP process on microstructural refurbishment in cast nickel-based superalloy, GTD-111. High Temper. Mater. Process. 26(2), 151–160 (2007)
A. Turazi, C.A. de Oliveira, C.E. Bohórquez et al., Study of GTD-111 superalloy microstructural evolution during high-temperature aging and after rejuvenation treatments. Metallogr. Microstruct. Anal. 4(1), 3–12 (2015)
K. Sabri, M.O. Si-Chaib, M. Gaceb, Lifetime extension prediction of the rejuvenated first stage gas turbine blades. Mater. Sci. Technol. 36(1), 46–54 (2020)
J. Liburdi, P. Lowden, D. Nagy, et al., Practical experience with the development of superalloy rejuvenation, in ASME Turbo Expo 2009: Power for Land, Sea, and Air. American Society of Mechanical Engineers Digital Collection, pp. 819–827 (2009)
K. Huang, K. Marthinsen, Q. Zhao, R.E. Logé, The double-edge effect of second-phase particles on the recrystallization behaviour and associated mechanical properties of metallic materials. Prog. Mater. Sci. 92, 284–359 (2018)
T. Wang, X. Wang, Z. Zhao et al., Dissolution behaviour of the γ′ precipitates in two kinds of Ni-based superalloys. Mater High Temper. 33(1), 51–57 (2016)
J. Wang, L. Zhou, L. Sheng et al., The microstructure evolution and its effect on the mechanical properties of a hot-corrosion resistant Ni-based superalloy during long-term thermal exposure. Mater. Des. 39, 55–62 (2012)
M. Aghaie-Khafri, M. Hajjavady, The effect of thermal exposure on the properties of a Ni-base superalloy. Mater. Sci. Eng. A 487(1–2), 388–393 (2008)
S. Atamert, J. Stekly, Microstructure, wear resistance, and stability of cobalt based and alternative iron based hard facing alloys. Surf. Eng. 9(3), 231–240 (1993)
A.K. Jena, M.C. Chaturvedi, The role of alloying elements in the design of nickel-base superalloys. J. Mater. Sci. 19(10), 3121–3139 (1984)
Y.Q. Chen, E. Francis, J. Robson et al., Compositional variations for small-scale gamma prime (γ′) precipitates formed at different cooling rates in an advanced Ni-based superalloy. Acta Mater. 85, 199–206 (2015) (Sajjadi SA, Zebarjad SM, Guthrie R, Isac M (2006) J Mater Process Technol 175:376–381)
X. Dong, X. Zhang, K. Du et al., Microstructure of carbides at grain boundaries in nickel based superalloys. J. Mater. Sci. Technol. 28(11), 1031–1038 (2012)
A. Glage, Nickel-based superalloys and their application in the aircraft industry. Ph.D. thesis, Università degli Studi di Trento (2007)
G.L. Erickson, Critical issues in the development of high temperature structural materials, ed. by N.S. Stoloff, D.J. Duquette, A.F. Giamei. Proceedings from the conference on critical issues in the development of high temperature structural materials, (TMS Publications, kona, hawaii, 7–14 Mar 1993), pp. 87–105
Danis Y (2008) Etude de la soudabilité d’un superalliage base nickel fortement chargé en éléments durcissants titane et aluminium: l’inconel 738. Thèse de doctorat, Bordeaux 1
M.J. Cieslak, G.A. Knorovsky, T.J. Headley et al., The solidification metallurgy of alloy 718 and other Nb-containing superalloys. Superalloy 718, 59–68 (1989)
C. Mons, Traitements thermiques des superalliages. Techniques de l'ingénieur. Matériaux métalliques, no M1165, pp. M1165.1–M1165.12 (1996)
F. Masoumi, M. Jahazi, D. Shahriari et al., Coarsening and dissolution of γ′ precipitates during solution treatment of AD730™ Ni-based superalloy: mechanisms and kinetics models. J. Alloys Compd. 658, 981–995 (2016)
J.M. Vitek, D.W. Gandy, S.S. Babu et al., Alloy Development of Nickel-Based Superalloy Weld Filler Metals Using Computational Thermodynamics (Oak Ridge National Laboratories, Oak Ridge, 2001)
J. Mao, Gamma prime precipitation modeling and strength responses in powder metallurgy superalloys. Graduate Theses, Dissertations, and Problem Reports. 1632. (2002)
M.A. Charpagne, T. Billot, J.M. Franchet et al., Heteroepitaxial recrystallization: a new mechanism discovered in a polycrystalline γ-γ′ nickel based superalloy. J. Alloys Compd. 688, 685–694 (2016)
G.E. Fuchs, Solution heat treatment response of a third generation single crystal Ni-base superalloy. Mater. Sci. Eng. A 300(1–2), 52–60 (2001)
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The authors whose names appear on the manuscript (Ouahid SIFI, Mohammed El Amine DJEGHLAL, Yamina MEBDOUA, Sofiane DJERAF, and Fayçal HADJ-LARBI) certify that they have no affiliation with an organization or entity having a financial interest, membership, employment, consultations.
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Sifi, O., Djeghlal, M.E., Mebdoua, Y. et al. The effect of the solution and aging treatments on the microstructures and microhardness of nickel-based superalloy. Appl. Phys. A 126, 345 (2020). https://doi.org/10.1007/s00339-020-03517-2
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DOI: https://doi.org/10.1007/s00339-020-03517-2